3-benzylamino-1-(tert-butyl-diphenyl-silanyloxy)-3-(tert-butyl-diphenyl-silanyloxymethyl)-heptan-2-ol

Base Information

Chemical Name:3-benzylamino-1-(tert-butyl-diphenyl-silanyloxy)-3-(tert-butyl-diphenyl-silanyloxymethyl)-heptan-2-ol
CAS No.:866925-83-9
Molecular Formula:C₄₇H₆₁NO₃Si₂
Molecular Weight:744.177
Hs Code.:

3-benzylamino-1-(<i>tert</i>-butyl-diphenyl-silanyloxy)-3-(<i>tert</i>-butyl-diphenyl-silanyloxymethyl)-heptan-2-ol

Synonyms:3-benzylamino-1-(tert-butyl-diphenyl-silanyloxy)-3-(tert-butyl-diphenyl-silanyloxymethyl)-heptan-2-ol

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Chemical Property of 3-benzylamino-1-(tert-butyl-diphenyl-silanyloxy)-3-(tert-butyl-diphenyl-silanyloxymethyl)-heptan-2-ol

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Technology Process of 3-benzylamino-1-(tert-butyl-diphenyl-silanyloxy)-3-(tert-butyl-diphenyl-silanyloxymethyl)-heptan-2-ol

There total 3 articles about 3-benzylamino-1-(tert-butyl-diphenyl-silanyloxy)-3-(tert-butyl-diphenyl-silanyloxymethyl)-heptan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 866925-79-3
(2R,3R)-3-Benzylamino-3-(tert-butyl-diphenyl-silanyloxymethyl)-heptane-1,2-diol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 866925-83-9
3-benzylamino-1-(tert-butyl-diphenyl-silanyloxy)-3-(tert-butyl-diphenyl-silanyloxymethyl)-heptan-2-ol

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetasy.2005.03.013

Reference yield:

: 866925-77-1
Benzyl-[(R)-1-(tert-butyl-diphenyl-silanyloxymethyl)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-pentyl]-amine

: 866925-83-9
3-benzylamino-1-(tert-butyl-diphenyl-silanyloxy)-3-(tert-butyl-diphenyl-silanyloxymethyl)-heptan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / HCl / methanol / 0.5 h / Heating

2: 72 percent / triethylamine; 4-(dimethylamino)pyridine / CH₂Cl₂ / 20 °C

With hydrogenchloride; dmap; triethylamine; In methanol; dichloromethane;
DOI:10.1016/j.tetasy.2005.03.013

Reference yield:

: 857293-90-4
C₃₀H₃₇NO₄Si

: 866925-83-9
3-benzylamino-1-(tert-butyl-diphenyl-silanyloxy)-3-(tert-butyl-diphenyl-silanyloxymethyl)-heptan-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: zinc bromide / diethyl ether / 0.25 h / cooling

1.2: diethyl ether / 5 h / -78 °C

2.1: 69 percent / Zn/Cu; acetic acid / 0.58 h / Heating

3.1: 82 percent / HCl / methanol / 0.5 h / Heating

4.1: 72 percent / triethylamine; 4-(dimethylamino)pyridine / CH₂Cl₂ / 20 °C

With hydrogenchloride; dmap; copper; acetic acid; triethylamine; zinc dibromide; zinc; In methanol; diethyl ether; dichloromethane;
DOI:10.1016/j.tetasy.2005.03.013