C₁₆H₁₈ClO₄P

Base Information

• Chemical Name: C₁₆H₁₈ClO₄P
• CAS No.: 1233656-30-8
• Molecular Formula: C₁₆H₁₈ClO₄P
• Molecular Weight: 340.743
• Mol file: 1233656-30-8.mol

Synonyms:C₁₆H₁₈ClO₄P

Chemical Property of C₁₆H₁₈ClO₄P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₁₈ClO₄P

There total 1 articles about C₁₆H₁₈ClO₄P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C9H12ClO3P (1233656-16-0) + para-Chlorobenzyl alcohol (873-76-7) → C16H18ClO4P (1233656-30-8)

Guidance literature:

With NMI; In dichloromethane; at 20 ℃; optical yield given as %de; Inert atmosphere;

DOI:10.1021/ol1006604

Reference yield:

morpholine (110-91-8,99108-56-2) + C16H18ClO4P (1233656-30-8) → 4-(4'-chloro-benzyl)morpholine (6425-43-0)

Guidance literature:

C₁₆H₁₈ClO₄P; With Grubbs catalyst first generation; In dichloromethane; at 50 ℃; Inert atmosphere;

morpholine; With tetra-(n-butyl)ammonium iodide; potassium carbonate; In chloroform; at 80 ℃; Inert atmosphere;

DOI:10.1021/ol1006604

Reference yield:

C12H16ClNO3S + C16H18ClO4P (1233656-30-8) → C19H21Cl2NO3S

Guidance literature:

C₁₆H₁₈ClO₄P; With Grubbs catalyst first generation; In dichloromethane; at 50 ℃; Inert atmosphere;

C₁₂H₁₆ClNO₃S; With tetra-(n-butyl)ammonium iodide; potassium carbonate; In tetrahydrofuran; at 80 ℃; Inert atmosphere;

DOI:10.1021/ol1006604

upstream raw materials:

C₉H₁₂ClO₃P

para-Chlorobenzyl alcohol

Downstream raw materials:

4-(4'-chloro-benzyl)morpholine

Refernces