Technology Process of C27H39N5O5S
There total 9 articles about C27H39N5O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrahydrofuran / 24 h / 20 °C
2: ammonium chloride; zinc / methanol / 2 h / Heating / reflux
3: triethylamine / tetrahydrofuran / 20 °C
4: hydrazine / ethanol / 1 h / 20 °C
5: 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / N,N-dimethyl-formamide / 4 h / 20 °C
With
ammonium chloride; triethylamine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; hydrazine; zinc;
In
tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18.5 h / 20 - 50 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -60 - -40 °C
2.2: -40 - 20 °C
3.1: 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / N,N-dimethyl-formamide / 4 h / 20 °C
With
n-butyllithium; N-ethyl-N,N-diisopropylamine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide;