Boc-Met-Glu-His-Phe-Pro-Gly-Pro

Base Information

Chemical Name:Boc-Met-Glu-His-Phe-Pro-Gly-Pro
CAS No.:92411-06-8
Molecular Formula:C₄₂H₅₉N₉O₁₂S
Molecular Weight:914.05
Hs Code.:

Synonyms:Boc-Met-Glu-His-Phe-Pro-Gly-Pro

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Chemical Property of Boc-Met-Glu-His-Phe-Pro-Gly-Pro

Chemical Property:

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Technology Process of Boc-Met-Glu-His-Phe-Pro-Gly-Pro

There total 11 articles about Boc-Met-Glu-His-Phe-Pro-Gly-Pro which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 92411-05-7
Boc-Met-γ-Bzl-Glu-His-Phe-Pro-Gly-Pro-OBzl

: 92411-06-8
Boc-Met-Glu-His-Phe-Pro-Gly-Pro

Guidance literature:: With cyclohexa-1,4-diene; palladium; In ethanol; for 2h; Heating;
DOI:10.1007/BF00769795

Reference yield:

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 92411-06-8
Boc-Met-Glu-His-Phe-Pro-Gly-Pro

Guidance literature:: Multi-step reaction with 8 steps

1: 53 percent / 1-hydroxybenzotriazole, N,N'-dicyclohexylcarbodiimide, triethylamine / tetrahydrofuran / 48 h / Ambient temperature

2: 100 percent / CH₂Cl₂ / 0.67 h / Ambient temperature

3: 70 percent / 1-hydroxybenzotriazole, N,N'-dicyclohexylcarbodiimide, triethylamine / tetrahydrofuran / 48 h / Ambient temperature

4: CH₂Cl₂ / Ambient temperature

5: 75 percent / 1-hydroxybenzotriazole, N,N'-dicyclohexylcarbodiimide, triethylamine / tetrahydrofuran / 48 h / Ambient temperature

6: CH₂Cl₂ / Ambient temperature

7: 1.) aq. H₂SO₄, 2.) 1-hydroxybenzotriazole, N,N'-dicyclohexylcarbodiimide, triethylamine / 2.) THF, room temp., 3 days

8: 76 percent / 1,4-cyclohexadiene / Pd-black / ethanol / 2 h / Heating

With cyclohexa-1,4-diene; sulfuric acid; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1007/BF00769795

Reference yield:

: 1738-78-9
L-phenylalanine benzyl ester p-toluene-sulfonic acid salt

: 92411-06-8
Boc-Met-Glu-His-Phe-Pro-Gly-Pro

Guidance literature:: Multi-step reaction with 8 steps

1: 88 percent / 1-hydroxybenzotriazole, N,N'-dicyclohexylcarbodiimide, triethylamine / tetrahydrofuran / 48 h / Ambient temperature

2: 93 percent / cyclohexene / Pd-black / ethanol / 1 h / Heating

3: 70 percent / 1-hydroxybenzotriazole, N,N'-dicyclohexylcarbodiimide, triethylamine / tetrahydrofuran / 48 h / Ambient temperature

4: CH₂Cl₂ / Ambient temperature

5: 75 percent / 1-hydroxybenzotriazole, N,N'-dicyclohexylcarbodiimide, triethylamine / tetrahydrofuran / 48 h / Ambient temperature

6: CH₂Cl₂ / Ambient temperature

7: 1.) aq. H₂SO₄, 2.) 1-hydroxybenzotriazole, N,N'-dicyclohexylcarbodiimide, triethylamine / 2.) THF, room temp., 3 days

8: 76 percent / 1,4-cyclohexadiene / Pd-black / ethanol / 2 h / Heating

With cyclohexa-1,4-diene; sulfuric acid; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; cyclohexene; palladium; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1007/BF00769795