methyl 3-((2S,3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-2-hydroxytetrahydro-2H-pyran-2-yl)propanenitrile

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Chemical Name:methyl 3-((2S,3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-2-hydroxytetrahydro-2H-pyran-2-yl)propanenitrile
CAS No.:1226983-42-1
Molecular Formula:C₃₇H₃₉NO₆
Molecular Weight:593.72
Hs Code.:

Synonyms:methyl 3-((2S,3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-2-hydroxytetrahydro-2H-pyran-2-yl)propanenitrile

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Chemical Property of methyl 3-((2S,3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-2-hydroxytetrahydro-2H-pyran-2-yl)propanenitrile

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Technology Process of methyl 3-((2S,3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-2-hydroxytetrahydro-2H-pyran-2-yl)propanenitrile

There total 1 articles about methyl 3-((2S,3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-2-hydroxytetrahydro-2H-pyran-2-yl)propanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 107-13-1,25014-41-9
acrylonitrile

: 89064-70-0
2,3,4,6-Tetra-O-benzyl-1-desoxy-1-nitro-D-glucopyranose

: 1226983-42-1
methyl 3-((2S,3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-2-hydroxytetrahydro-2H-pyran-2-yl)propanenitrile

Guidance literature:: acrylonitrile; 2,3,4,6-Tetra-O-benzyl-1-desoxy-1-nitro-D-glucopyranose; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 10 ℃; for 0.5h;

With silica gel; Hydrolysis; Column chromatography;
DOI:10.1016/j.tetlet.2010.03.003