4,4-difluoro-4-bora-3a,4a-diaza-3-amino-8-(4-methoxyphenyl)-s-indacene

Base Information

Chemical Name:4,4-difluoro-4-bora-3a,4a-diaza-3-amino-8-(4-methoxyphenyl)-s-indacene
CAS No.:1529762-50-2
Molecular Formula:C₁₆H₁₄BF₂N₃O
Molecular Weight:313.114
Hs Code.:

Synonyms:4,4-difluoro-4-bora-3a,4a-diaza-3-amino-8-(4-methoxyphenyl)-s-indacene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4-difluoro-4-bora-3a,4a-diaza-3-amino-8-(4-methoxyphenyl)-s-indacene

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Technology Process of 4,4-difluoro-4-bora-3a,4a-diaza-3-amino-8-(4-methoxyphenyl)-s-indacene

There total 3 articles about 4,4-difluoro-4-bora-3a,4a-diaza-3-amino-8-(4-methoxyphenyl)-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1529762-65-9
C₃₄H₂₇BF₂N₃OP

: 1529762-50-2
4,4-difluoro-4-bora-3a,4a-diaza-3-amino-8-(4-methoxyphenyl)-s-indacene

Guidance literature:: With water; In tetrahydrofuran; Reflux;
DOI:10.1016/j.dyepig.2013.10.038

Reference yield:

: 1314661-35-2
3-bromo-4,4-difluoro-8-(4-methoxyphenyl)-4-bora-3a,4a-diaza-s-indacene

: 1529762-50-2
4,4-difluoro-4-bora-3a,4a-diaza-3-amino-8-(4-methoxyphenyl)-s-indacene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / acetonitrile / 4 h / 20 °C

2: triphenylphosphine; water

With sodium azide; water; triphenylphosphine; In acetonitrile; 2: |Staudinger Azide Reduction;
DOI:10.1016/j.dyepig.2013.10.038