tricyclohexyl-methylenephosphorane

Base Information

• Chemical Name: tricyclohexyl-methylenephosphorane
• CAS No.: 29219-31-6
• Molecular Formula: C₁₉H₃₅P
• Molecular Weight: 294.461

Synonyms:tricyclohexyl-methylenephosphorane

Chemical Property of tricyclohexyl-methylenephosphorane

Chemical Property:

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Technology Process of tricyclohexyl-methylenephosphorane

There total 2 articles about tricyclohexyl-methylenephosphorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

Tricyclohexyl-methyl-phosphonium; bromide (99019-79-1) → tricyclohexyl-methylenephosphorane (29219-31-6)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane;

DOI:10.1016/0040-4020(80)80204-3

Reference yield:

→ tricyclohexyl-methylenephosphorane (29219-31-6)

Guidance literature:

Tricyclohexylphosphin, Dibrom-methan in Dioxan;

Reference yield: 72.0%

bis(η5:η1-adamantylidenepentafulvene)titanium + tricyclohexyl-methylenephosphorane (29219-31-6) → C49H71PTi

Guidance literature:

In hexane; at 20 ℃; for 16h; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.organomet.8b00831

upstream raw materials:

Tricyclohexyl-methyl-phosphonium; bromide

Downstream raw materials:

(CO)3NiCH₂P(C₆H₁₁-cyclo)3

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