C₃₁H₃₈N₂O₆

Base Information

Chemical Name:C₃₁H₃₈N₂O₆
CAS No.:1613625-68-5
Molecular Formula:C₃₁H₃₈N₂O₆
Molecular Weight:534.653
Hs Code.:

C<sub>31</sub>H<sub>38</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:C₃₁H₃₈N₂O₆

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Chemical Property of C₃₁H₃₈N₂O₆

Chemical Property:

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Technology Process of C₃₁H₃₈N₂O₆

There total 18 articles about C₃₁H₃₈N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1613625-67-4
C₂₀H₂₆F₃NO₇S

: 149965-78-6
N-benzyloxycarbonyl-but-3-ynyl-1-amine

: 1613625-68-5
C₃₁H₃₈N₂O₆

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; triethylamine; In hexane; acetonitrile; for 4h; Inert atmosphere; Reflux;

Reference yield:

: 70179-57-6
β-(8-methoxy-1,2,3,4-tetrahydro-5-naphthyl)-propionic acid

: 1613625-68-5
C₃₁H₃₈N₂O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: pivaloyl chloride; triethylamine / tetrahydrofuran / 0.67 h / -10 °C

2.1: lithium chloride / tetrahydrofuran / 12 h / 20 °C

3.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C

3.2: -78 °C

3.3: 16 h / -78 - 27 °C

4.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 3 h / 0 °C

5.1: hydrogen; palladium 10% on activated carbon / water / 12 h / 20 °C / 760.05 Torr

6.1: acetic acid; hydrogen bromide / 4 h / Reflux

7.1: acetyl chloride / 4 h / 0 °C / Reflux

8.1: sodium hydrogencarbonate / methanol; water / 3 h / 0 - 20 °C

9.1: pyridine / 2 h / 0 - 20 °C

10.1: tri-tert-butyl phosphine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / acetonitrile; hexane / 4 h / Inert atmosphere; Reflux

With pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; hydrogen bromide; hydrogen; dihydrogen peroxide; pivaloyl chloride; potassium hexamethylsilazane; sodium hydrogencarbonate; acetic acid; triethylamine; acetyl chloride; lithium chloride; lithium hydroxide; In tetrahydrofuran; methanol; hexane; water; acetonitrile;

Reference yield:

: 1613625-63-0
C₁₄H₁₇N₃O₃

: 1613625-68-5
C₃₁H₃₈N₂O₆

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogen; palladium 10% on activated carbon / water / 12 h / 20 °C / 760.05 Torr

2: acetic acid; hydrogen bromide / 4 h / Reflux

3: acetyl chloride / 4 h / 0 °C / Reflux

4: sodium hydrogencarbonate / methanol; water / 3 h / 0 - 20 °C

5: pyridine / 2 h / 0 - 20 °C

6: tri-tert-butyl phosphine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / acetonitrile; hexane / 4 h / Inert atmosphere; Reflux

With pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; hydrogen bromide; hydrogen; sodium hydrogencarbonate; acetic acid; triethylamine; acetyl chloride; In methanol; hexane; water; acetonitrile;