C₃₈H₃₂N₄O

Base Information

Chemical Name:C₃₈H₃₂N₄O
CAS No.:1049634-23-2
Molecular Formula:C₃₈H₃₂N₄O
Molecular Weight:560.698
Hs Code.:

C<sub>38</sub>H<sub>32</sub>N<sub>4</sub>O

Synonyms:C₃₈H₃₂N₄O

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Chemical Property of C₃₈H₃₂N₄O

Chemical Property:

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Technology Process of C₃₈H₃₂N₄O

There total 9 articles about C₃₈H₃₂N₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1049634-22-1
C₄₀H₃₄N₄O₂

: 1049634-23-2
C₃₈H₃₂N₄O

Guidance literature:: With sodium hydroxide; ethanol; water; at 120 ℃; for 0.416667h; Microwave irradiation;

Reference yield:

: 6602-32-0
2-bromo-pyridin-3-ol

: 1049634-23-2
C₃₈H₃₂N₄O

Guidance literature:: Multi-step reaction with 11 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 °C / Heating / reflux

2.1: tetraethylammonium chloride; potassium acetate / palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 105 °C

3.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide; tert-butyl alcohol / dichloromethane / 20 °C

4.1: sodium periodate / tetrahydrofuran; water / 2.5 h / 20 °C

5.1: sodium tetrahydroborate / methanol / 20 °C

5.2: 0.5 h

6.1: phosphorus tribromide / chloroform / 3.5 h / Heating / reflux

6.2: 0 °C

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

8.1: 2,6-dimethylpyridine; oxalyl dichloride / dichloromethane / 0.5 h / 0 °C

8.2: 2.5 h / 0 - 20 °C

9.1: acetonitrile / 60 h / Heating / reflux

10.1: lithium hexamethyldisilazane / tetrahydrofuran / 3 h / -78 - -65 °C

10.2: -65 °C

11.1: sodium hydroxide; ethanol; water / 0.42 h / 120 °C / Microwave irradiation

With 2,6-dimethylpyridine; sodium hydroxide; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; oxalyl dichloride; ethanol; di-isopropyl azodicarboxylate; tetraethylammonium chloride; water; potassium acetate; phosphorus tribromide; 4-methylmorpholine N-oxide; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; lithium hexamethyldisilazane; tert-butyl alcohol; palladium diacetate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetonitrile; 1.1: Mitsunobu reaction / 2.1: Intramolecular Heck cyclization;

Reference yield:

: 405174-45-0
2-bromo-3-(but-3-en-1-yloxy)pyridine

: 1049634-23-2
C₃₈H₃₂N₄O

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetraethylammonium chloride; potassium acetate / palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 105 °C

2.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide; tert-butyl alcohol / dichloromethane / 20 °C

3.1: sodium periodate / tetrahydrofuran; water / 2.5 h / 20 °C

4.1: sodium tetrahydroborate / methanol / 20 °C

4.2: 0.5 h

5.1: phosphorus tribromide / chloroform / 3.5 h / Heating / reflux

5.2: 0 °C

6.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

7.1: 2,6-dimethylpyridine; oxalyl dichloride / dichloromethane / 0.5 h / 0 °C

7.2: 2.5 h / 0 - 20 °C

8.1: acetonitrile / 60 h / Heating / reflux

9.1: lithium hexamethyldisilazane / tetrahydrofuran / 3 h / -78 - -65 °C

9.2: -65 °C

10.1: sodium hydroxide; ethanol; water / 0.42 h / 120 °C / Microwave irradiation

With 2,6-dimethylpyridine; sodium hydroxide; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; oxalyl dichloride; ethanol; tetraethylammonium chloride; water; potassium acetate; phosphorus tribromide; 4-methylmorpholine N-oxide; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane; tert-butyl alcohol; palladium diacetate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetonitrile; 1.1: Intramolecular Heck cyclization;