phenyl 2,3,4-O-triacetyl-1-thio-β-D-lyxopyranoside

Base Information

Chemical Name:phenyl 2,3,4-O-triacetyl-1-thio-β-D-lyxopyranoside
CAS No.:1593691-70-3
Molecular Formula:C₁₇H₂₀O₇S
Molecular Weight:368.408
Hs Code.:

Synonyms:phenyl 2,3,4-O-triacetyl-1-thio-β-D-lyxopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 2,3,4-O-triacetyl-1-thio-β-D-lyxopyranoside

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Technology Process of phenyl 2,3,4-O-triacetyl-1-thio-β-D-lyxopyranoside

There total 2 articles about phenyl 2,3,4-O-triacetyl-1-thio-β-D-lyxopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 108-98-5
thiophenol

: 4099-16-5
2,3,4-tri-O-acetyl-α-D-lyxopyranosyl bromide

: 1593691-70-3
phenyl 2,3,4-O-triacetyl-1-thio-β-D-lyxopyranoside

Guidance literature:: With tetra(n-butyl)ammonium hydrogensulfate; sodium carbonate; In water; ethyl acetate; at 20 ℃; for 1.08333h; Inert atmosphere;
DOI:10.1021/acs.joc.8b02037

Reference yield:

: 151908-65-5
1,2,3,4-Tetra-O-acetyl-D-lyxopyranose

: 108-98-5
thiophenol

: 1593691-65-6
phenyl 2,3,4-tri-O-acetyl-1-thio-D-lyxopyranoside

: 1593691-70-3
phenyl 2,3,4-O-triacetyl-1-thio-β-D-lyxopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; for 18h; Overall yield = 87%; Overall yield = 1.1 g; Inert atmosphere;
DOI:10.1002/anie.201310569