Technology Process of C13H15ClO2
There total 3 articles about C13H15ClO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
thionyl chloride;
In
1,2-dichloro-ethane; benzene;
at 0 ℃;
for 5h;
Inert atmosphere;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1-ethyl-piperidine; tin(II) trifluoromethanesulfonate / 1,2-dichloro-ethane / 1 h / 0 °C / Inert atmosphere
1.2: Inert atmosphere; Reflux
2.1: sodium hydroxide; water / ethanol / 5 h / 20 °C
3.1: thionyl chloride / benzene; 1,2-dichloro-ethane / 5 h / 0 °C / Inert atmosphere; Reflux
With
1-ethyl-piperidine; tin(II) trifluoromethanesulfonate; thionyl chloride; water; sodium hydroxide;
In
ethanol; 1,2-dichloro-ethane; benzene;
1.1: Horner-Wadsworth-Emmons Olefination / 1.2: Horner-Wadsworth-Emmons Olefination;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydroxide; water / ethanol / 5 h / 20 °C
2: thionyl chloride / benzene; 1,2-dichloro-ethane / 5 h / 0 °C / Inert atmosphere; Reflux
With
thionyl chloride; water; sodium hydroxide;
In
ethanol; 1,2-dichloro-ethane; benzene;