(1R,2S,5R)-8-phenylmenthyl (E)-5-[(tetrahydro-2H-pyran-2-yl)oxy]-2-pentenoate

Base Information

Chemical Name:(1R,2S,5R)-8-phenylmenthyl (E)-5-[(tetrahydro-2H-pyran-2-yl)oxy]-2-pentenoate
CAS No.:318268-10-9
Molecular Formula:C₂₆H₃₈O₄
Molecular Weight:414.585
Hs Code.:

Synonyms:(1R,2S,5R)-8-phenylmenthyl (E)-5-[(tetrahydro-2H-pyran-2-yl)oxy]-2-pentenoate

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Chemical Property of (1R,2S,5R)-8-phenylmenthyl (E)-5-[(tetrahydro-2H-pyran-2-yl)oxy]-2-pentenoate

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Technology Process of (1R,2S,5R)-8-phenylmenthyl (E)-5-[(tetrahydro-2H-pyran-2-yl)oxy]-2-pentenoate

There total 1 articles about (1R,2S,5R)-8-phenylmenthyl (E)-5-[(tetrahydro-2H-pyran-2-yl)oxy]-2-pentenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 62592-78-3
3-(2-tetrahydropyranyloxy)propanal

: 113368-89-1
(-)-8-phenylmenthyl dimethyl phosphonoacetate

: 318268-10-9
(1R,2S,5R)-8-phenylmenthyl (E)-5-[(tetrahydro-2H-pyran-2-yl)oxy]-2-pentenoate

Guidance literature:: With sodium hydride; In tetrahydrofuran;
DOI:10.1002/1099-0690(200011)2000:21<3595::AID-EJOC3595>3.0.CO;2-N

Reference yield: 75.0%

: 318268-10-9
(1R,2S,5R)-8-phenylmenthyl (E)-5-[(tetrahydro-2H-pyran-2-yl)oxy]-2-pentenoate

: 205692-50-8
(1R,2S,5R)-8-phenylmenthyl (E)-5-hydroxy-2-pentenoate

Guidance literature:: With Amberlyst 15; In methanol; at 40 ℃; for 6.5h;
DOI:10.1002/1099-0690(200011)2000:21<3595::AID-EJOC3595>3.0.CO;2-N

Reference yield:

: 318268-10-9
(1R,2S,5R)-8-phenylmenthyl (E)-5-[(tetrahydro-2H-pyran-2-yl)oxy]-2-pentenoate

: 318268-16-5
(1R,2S,5R)-8-phenylmenthyl (E)-5-[(methylsulfonyl)oxy]-2-pentenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Amberlyst 15 / methanol / 6.5 h / 40 °C

2: 99 percent / triethylamine / CH₂Cl₂ / 1.5 h / 20 °C

With Amberlyst 15; triethylamine; In methanol; dichloromethane; 1: Hydrolysis / 2: mesylation;
DOI:10.1002/1099-0690(200011)2000:21<3595::AID-EJOC3595>3.0.CO;2-N