1-Chloro-3-methylpyrido[1,2-a]benzimidazole-4-carbonitrile

Base Information

Chemical Name:1-Chloro-3-methylpyrido[1,2-a]benzimidazole-4-carbonitrile
CAS No.:121105-78-0
Molecular Formula:C₁₃H₈ClN₃
Molecular Weight:241.68
Hs Code.:2933990090
NSC Number:610507
DSSTox Substance ID:DTXSID30326705
Wikidata:Q82087867
ChEMBL ID:CHEMBL1348803
Mol file:121105-78-0.mol

Synonyms:121105-78-0;1-Chloro-3-methylpyrido[1,2-a]benzimidazole-4-carbonitrile;1-chloro-3-methylbenzo[4,5]imidazo[1,2-a]pyridine-4-carbonitrile;1-Chloro-3-methyl-benzo[4,5]imidazo[1,2-a]pyridine-4-carbonitrile;MLS000708330;SMR000287797;1-CHLORO-3-METHYL-BENZO(4,5)IMIDAZO(1,2-A)PYRIDINE-4-CARBONITRILE;NSC610507;ETHYL3-BUTENOATE;Oprea1_006254;Oprea1_398722;cid_355876;SCHEMBL2162680;CHEMBL1348803;BDBM68125;DTXSID30326705;HMS2715E21;WEA10578;BBL012348;MFCD00649385;STK105094;AKOS000561786;NSC-610507;VS-03293;BB 0219298;CS-0219764;EN300-04882;J-504510;Z56899195;1-chloro-3-methyl-4-pyrido[1,2-a]benzimidazolecarbonitrile;1-chloranyl-3-methyl-pyrido[1,2-a]benzimidazole-4-carbonitrile;1-chloro-3-methyl-pyrido[1,2-a]benzimidazole-4-carbonitrile;1-Chloro-3-methylpyrido[1,2-a]benzimidazole-4-carbonitrile #;Pyrido[1,2-a]benzimidazole-4-carbonitrile, 1-chloro-3-methyl-;4-CHLORO-2-METHYLBENZO[4,5]IMIDAZO[1,2-A]PYRIDIN-1-YL CYANIDE;13-CHLORO-11-METHYL-1,8-DIAZATRICYCLO[7.4.0.0(2),?]TRIDECA-2(7),3,5,8,10,12-HEXAENE-10-CARBONITRILE;13-chloro-11-methyl-1,8-diazatricyclo[7.4.0.0,2,7]trideca-2,4,6,8,10,12-hexaene-10-carbonitrile

Suppliers and Price of 1-Chloro-3-methylpyrido[1,2-a]benzimidazole-4-carbonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-Chloro-3-methylbenzo[4,5]imidazo[1,2-a]pyridine-4-carbonitrile
50mg
$ 45.00

American Custom Chemicals Corporation
1-CHLORO-3-METHYL-BENZO[4,5]IMIDAZO[1,2-A]PYRIDINE-4-CARBONITRILE 95.00%
2.5G
$ 1065.66

American Custom Chemicals Corporation
1-CHLORO-3-METHYL-BENZO[4,5]IMIDAZO[1,2-A]PYRIDINE-4-CARBONITRILE 95.00%
1G
$ 765.23

American Custom Chemicals Corporation
1-CHLORO-3-METHYL-BENZO[4,5]IMIDAZO[1,2-A]PYRIDINE-4-CARBONITRILE 95.00%
5G
$ 1295.03

AK Scientific
1-Chloro-3-methyl-benzo[4,5]imidazo[1,2-a]pyridine-4-carbonitrile
5g
$ 1100.00

Total 8 raw suppliers

Chemical Property of 1-Chloro-3-methylpyrido[1,2-a]benzimidazole-4-carbonitrile

Chemical Property:

Refractive Index:1.696
Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：41.09000
Density:1.36g/cm³
LogP:3.32098
XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:241.0406750
Heavy Atom Count:17
Complexity:350

Purity/Quality:

97% ^*data from raw suppliers

1-Chloro-3-methylbenzo[4,5]imidazo[1,2-a]pyridine-4-carbonitrile ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C2=NC3=CC=CC=C3N2C(=C1)Cl)C#N

Technology Process of 1-Chloro-3-methylpyrido[1,2-a]benzimidazole-4-carbonitrile

There total 2 articles about 1-Chloro-3-methylpyrido[1,2-a]benzimidazole-4-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 60792-57-6
3-methyl-1-oxo-1H,5H-pyrido<1,2-a>benzimidazole-4-carbonitrile

: 121105-78-0
1-chloro-3-methylpyrido<1,2-a>benzimidazole-4-carbonitrile

Guidance literature:: With trichlorophosphate; for 1h; Heating;
DOI:10.1002/jhet.5570250622

Reference yield:

: 4414-88-4
1H-benzimidazol-2-acetonitrile

: 121105-78-0
1-chloro-3-methylpyrido<1,2-a>benzimidazole-4-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / ammonium acetate / 0.75 h / 140 - 150 °C

2: 93 percent / phosphorus oxychloride / 1 h / Heating

With ammonium acetate; trichlorophosphate;
DOI:10.1002/jhet.5570250622

Reference yield:

: 121105-78-0
1-chloro-3-methylpyrido<1,2-a>benzimidazole-4-carbonitrile

: 121105-81-5
3-methyl-1-(triphenylphosphoranylideneamino)pyrido<1,2-a>benzimidazole-4-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / sodium azide / dimethylformamide / 0.5 h / Ambient temperature

2: benzene / 45 h / Ambient temperature

With sodium azide; In N,N-dimethyl-formamide; benzene;
DOI:10.1002/jhet.5570250622