7(R)-[(S)-(p-methoxybenzyloxy)benzyl]-6(R)-(t-butyldiphenylsilyloxy)-4,5-didehydro-2-oxepanone

Base Information

Chemical Name:7(R)-[(S)-(p-methoxybenzyloxy)benzyl]-6(R)-(t-butyldiphenylsilyloxy)-4,5-didehydro-2-oxepanone
CAS No.:1005208-33-2
Molecular Formula:C₃₇H₄₀O₅Si
Molecular Weight:592.807
Hs Code.:

Synonyms:7(R)-[(S)-(p-methoxybenzyloxy)benzyl]-6(R)-(t-butyldiphenylsilyloxy)-4,5-didehydro-2-oxepanone

Suppliers and Price of 7(R)-[(S)-(p-methoxybenzyloxy)benzyl]-6(R)-(t-butyldiphenylsilyloxy)-4,5-didehydro-2-oxepanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7(R)-[(S)-(p-methoxybenzyloxy)benzyl]-6(R)-(t-butyldiphenylsilyloxy)-4,5-didehydro-2-oxepanone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7(R)-[(S)-(p-methoxybenzyloxy)benzyl]-6(R)-(t-butyldiphenylsilyloxy)-4,5-didehydro-2-oxepanone

There total 1 articles about 7(R)-[(S)-(p-methoxybenzyloxy)benzyl]-6(R)-(t-butyldiphenylsilyloxy)-4,5-didehydro-2-oxepanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1005208-31-0
5-C-phenyl-5-O-(p-methoxybenzyl)-3-O-(t-butyldiphenylsilyl)-L-xylo-pent-1-en-3,5-diol-4-yl 3-butenoate

: 1005208-33-2
7(R)-[(S)-(p-methoxybenzyloxy)benzyl]-6(R)-(t-butyldiphenylsilyloxy)-4,5-didehydro-2-oxepanone

Guidance literature:: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In benzene; at 80 ℃; for 11h;
DOI:10.1039/b713070h

Reference yield: 95.0%

: 1005208-33-2
7(R)-[(S)-(p-methoxybenzyloxy)benzyl]-6(R)-(t-butyldiphenylsilyloxy)-4,5-didehydro-2-oxepanone

: 1005208-39-8
7(R)-[(S)-(hydroxy)benzyl]-6(R)-(t-butyldiphenylsilyloxy)-4,5-didehydro-2-oxepanone

Guidance literature:: With trityl tetrafluoroborate; In dichloromethane; at 25 ℃; for 0.00833333h;
DOI:10.1039/b713070h

Reference yield:

: 1005208-33-2
7(R)-[(S)-(p-methoxybenzyloxy)benzyl]-6(R)-(t-butyldiphenylsilyloxy)-4,5-didehydro-2-oxepanone

: 1005208-35-4
7(R)-[(S)-(p-methoxybenzyloxy)benzyl]-6(R)-(t-butyldiphenylsilyloxy)-5(S)-hydroxy-3,4-didehydro-2-oxepanone

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 45 ℃; for 48h;
DOI:10.1039/b713070h