Technology Process of ethyl cis-2-cyclopentylacetate
There total 7 articles about ethyl cis-2-cyclopentylacetate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride;
In
benzene;
for 8h;
Heating;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 75 percent / aq. sodium hydroxide / tetrahydrofuran / 12 h
2: 100 percent / LAH / diethyl ether; tetrahydrofuran / 15 h / Heating
3: 54 percent / aq. NaOH / tetrahydrofuran / 12 h
4: ozone / CH2Cl2; methanol / -78 °C
5: NaH / tetrahydrofuran / 5 h
6: 84 percent / Bu3SnH, AIBN / benzene / 8 h / Heating
With
sodium hydroxide; lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; ozone;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; benzene;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: oxalyl dichloride / benzene / 12 h
2: 75 percent / aq. sodium hydroxide / tetrahydrofuran / 12 h
3: 100 percent / LAH / diethyl ether; tetrahydrofuran / 15 h / Heating
4: 54 percent / aq. NaOH / tetrahydrofuran / 12 h
5: ozone / CH2Cl2; methanol / -78 °C
6: NaH / tetrahydrofuran / 5 h
7: 84 percent / Bu3SnH, AIBN / benzene / 8 h / Heating
With
sodium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; ozone;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; benzene;
