N₁,N₁-dibenzyl-N₁₈-octadecyl-3,6,12,15-tetraoxa-8,17-dioxo-9,18-diaza-esatriacontylamine

Base Information

• Chemical Name: N₁,N₁-dibenzyl-N₁₈-octadecyl-3,6,12,15-tetraoxa-8,17-dioxo-9,18-diaza-esatriacontylamine
• CAS No.: 1301620-84-7
• Molecular Formula: C₆₂H₁₀₉N₃O₆
• Molecular Weight: 992.564

Synonyms:N₁,N₁-dibenzyl-N₁₈-octadecyl-3,6,12,15-tetraoxa-8,17-dioxo-9,18-diaza-esatriacontylamine

Chemical Property of N₁,N₁-dibenzyl-N₁₈-octadecyl-3,6,12,15-tetraoxa-8,17-dioxo-9,18-diaza-esatriacontylamine

Chemical Property:

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Technology Process of N₁,N₁-dibenzyl-N₁₈-octadecyl-3,6,12,15-tetraoxa-8,17-dioxo-9,18-diaza-esatriacontylamine

There total 4 articles about N₁,N₁-dibenzyl-N₁₈-octadecyl-3,6,12,15-tetraoxa-8,17-dioxo-9,18-diaza-esatriacontylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

[2-(2-dibenzylaminoethoxy)ethoxy]acetic acid (166108-70-9) + N9-octadecyl-3,6-dioxa-8-oxo-9-aza-heptacosylamine (1301620-83-6) → N1,N1-dibenzyl-N18-octadecyl-3,6,12,15-tetraoxa-8,17-dioxo-9,18-diaza-esatriacontylamine (1301620-84-7)

Guidance literature:

With O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In chloroform;

DOI:10.1039/c1cc10172b

Reference yield:

[2-(2-dibenzylaminoethoxy)ethoxy]acetic acid (166108-70-9) → N1,N1-dibenzyl-N18-octadecyl-3,6,12,15-tetraoxa-8,17-dioxo-9,18-diaza-esatriacontylamine (1301620-84-7)

Guidance literature:

Multi-step reaction with 3 steps

1: O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / chloroform

2: palladium on carbon; hydrogen / tetrahydrofuran / 14 h

3: O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / chloroform

With O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; palladium on carbon; hydrogen; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; chloroform;

DOI:10.1039/c1cc10172b

Reference yield:

N1,N1-dibenzyl-N9-octadecyl-3,6-dioxa-8-oxo-9-azaheptacosylamine (1301620-82-5) → N1,N1-dibenzyl-N18-octadecyl-3,6,12,15-tetraoxa-8,17-dioxo-9,18-diaza-esatriacontylamine (1301620-84-7)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium on carbon; hydrogen / tetrahydrofuran / 14 h

2: O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / chloroform

With O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; palladium on carbon; hydrogen; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; chloroform;

DOI:10.1039/c1cc10172b

upstream raw materials:

[2-(2-dibenzylaminoethoxy)ethoxy]acetic acid

N₉-octadecyl-3,6-dioxa-8-oxo-9-aza-heptacosylamine

N₁,N₁-dibenzyl-N₉-octadecyl-3,6-dioxa-8-oxo-9-azaheptacosylamine

benzyl bromide

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