Technology Process of C25H36IN5O4
There total 4 articles about C25H36IN5O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(1S,2S,3S,5R)-(+)-isopinocampheylamine;
With
diisobutylaluminium hydride;
In
tetrahydrofuran; toluene;
at 0 ℃;
for 2h;
C16H20BrNO5;
In
tetrahydrofuran; toluene;
for 2h;
With
Rochelle's salt;
In
tetrahydrofuran; water; toluene;
for 5h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
1.2: 1 h
2.1: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C
3.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / 0 °C
3.2: 2 h
3.3: 5 h
With
titanium(IV) isopropylate; diisobutylaluminium hydride; pyridine hydrogenfluoride;
In
tetrahydrofuran; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2
1.2: pH 7 / Alkaline aqueous solution
2.1: benzene / Heating / reflux
3.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
3.2: 1 h
4.1: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C
5.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / 0 °C
5.2: 2 h
5.3: 5 h
With
titanium(IV) isopropylate; hydrogenchloride; methyl orange; diisobutylaluminium hydride; sodium cyanoborohydride; pyridine hydrogenfluoride;
In
tetrahydrofuran; methanol; water; toluene; benzene;
