C₂₁H₃₆O₅Si

Base Information

Chemical Name:C₂₁H₃₆O₅Si
CAS No.:1448551-45-8
Molecular Formula:C₂₁H₃₆O₅Si
Molecular Weight:396.599
Hs Code.:

C<sub>21</sub>H<sub>36</sub>O<sub>5</sub>Si

Synonyms:C₂₁H₃₆O₅Si

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Chemical Property of C₂₁H₃₆O₅Si

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Technology Process of C₂₁H₃₆O₅Si

There total 3 articles about C₂₁H₃₆O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: tert-butyl(((3S,4R)-1-((3,4-dimethoxybenzyl)oxy)-4-methylhex-5-en-3-yl)oxy)dimethylsilane

: 1448551-45-8
C₂₁H₃₆O₅Si

Guidance literature:: tert-butyl(((3S,4R)-1-((3,4-dimethoxybenzyl)oxy)-4-methylhex-5-en-3-yl)oxy)dimethylsilane; With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; tert-butyl alcohol; at 23 ℃; for 7h;

With sodium periodate; In tetrahydrofuran; water; tert-butyl alcohol; for 2h;
DOI:10.1002/anie.201302535

Reference yield:

: 144681-75-4
3-<(3,4-Dimethoxyphenyl)methoxy>propanal

: 1448551-45-8
C₂₁H₃₆O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate; n-butyllithium / tetrahydrofuran / 0.17 h / -45 °C

1.2: 0.5 h / -78 °C

2.1: 1H-imidazole / dichloromethane; N,N-dimethyl-formamide

3.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 7 h / 23 °C

3.2: 2 h

With 1H-imidazole; osmium(VIII) oxide; n-butyllithium; potassium tert-butylate; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/anie.201302535

Reference yield:

: (3S,4R)-1-((3,4-dimethoxybenzyl)oxy)-4-methylhex-5-en-3-ol

: 1448551-45-8
C₂₁H₃₆O₅Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / dichloromethane; N,N-dimethyl-formamide

2.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 7 h / 23 °C

2.2: 2 h

With 1H-imidazole; osmium(VIII) oxide; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/anie.201302535