6-O-(triphenylmethyl)-β-D-glucopyranosyl-6'-O-(triphenylmethyl)-β-D-glucopyranoside

Base Information

• Chemical Name: 6-O-(triphenylmethyl)-β-D-glucopyranosyl-6'-O-(triphenylmethyl)-β-D-glucopyranoside
• CAS No.: 108811-30-9
• Molecular Formula: C₅₀H₅₀O₁₁
• Molecular Weight: 826.94
• Mol file: 108811-30-9.mol

Synonyms:6-O-(triphenylmethyl)-β-D-glucopyranosyl-6'-O-(triphenylmethyl)-β-D-glucopyranoside

Chemical Property of 6-O-(triphenylmethyl)-β-D-glucopyranosyl-6'-O-(triphenylmethyl)-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-O-(triphenylmethyl)-β-D-glucopyranosyl-6'-O-(triphenylmethyl)-β-D-glucopyranoside

There total 5 articles about 6-O-(triphenylmethyl)-β-D-glucopyranosyl-6'-O-(triphenylmethyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

TREHALOSE (99-20-7) + trityl chloride (76-83-5) → 6-O-(triphenylmethyl)-α-D-glucopyranosyl-6'-O-(triphenylmethyl)-α-D-glucopyranoside (50705-44-7,108811-30-9)

Guidance literature:

With pyridine; at 20 - 40 ℃; for 20h; Inert atmosphere;

DOI:10.1021/acs.orglett.9b01725

Reference yield: 100.0%

2,2',3,3',4,4'-hexa-O-acetyl-6,6'-di-O-trityl-α,α-trehalose (75869-80-6) → 6-O-(triphenylmethyl)-α-D-glucopyranosyl-6'-O-(triphenylmethyl)-α-D-glucopyranoside (50705-44-7,108811-30-9)

Guidance literature:

With methanol; sodium methylate; In tetrahydrofuran; for 120h; Inert atmosphere; Reflux;

DOI:10.1016/j.carres.2012.05.014

Reference yield: 92.0%

trityl chloride (76-83-5) + trehalose dihydrate (6138-23-4,138858-75-0) → triphenylmethyl alcohol (76-84-6) + 6-O-(triphenylmethyl)-α-D-glucopyranosyl-6'-O-(triphenylmethyl)-α-D-glucopyranoside (50705-44-7,108811-30-9)

Guidance literature:

In pyridine; for 45h; Ambient temperature;

DOI:10.1016/S0008-6215(00)85440-3

upstream raw materials:

TREHALOSE

trityl chloride

trehalose dihydrate

2,2',3,3',4,4'-hexa-O-acetyl-6,6'-di-O-trityl-α,α-trehalose

Downstream raw materials:

2,3,4-tri-O-methyl-6-O-(triphenylmethyl) β-D-glucopyranosyl-2'-3'-4'-tri-O-methyl-6'-O-(triphenylmethyl)-β-D-glucopyranoside

2,3,4,2',3',4'-hexa-O-benzyl-6,6'-di-O-trityl-β,β-trehalose

2,3,4,2',3',4'-hexa-O-benzyl-6,6'-di-O-trityl-α,α-trehalose

2,2',3,3',4,4'-hexa-O-acetyl-6,6'-di-O-trityl-α,α-trehalose