2,2-dimethylpent-4-enylcarbamic acid benzyl ester

Base Information

• Chemical Name: 2,2-dimethylpent-4-enylcarbamic acid benzyl ester
• CAS No.: 886576-63-2
• Molecular Formula: C₁₅H₂₁NO₂
• Molecular Weight: 247.337

Synonyms:2,2-dimethylpent-4-enylcarbamic acid benzyl ester

Chemical Property of 2,2-dimethylpent-4-enylcarbamic acid benzyl ester

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

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Technology Process of 2,2-dimethylpent-4-enylcarbamic acid benzyl ester

There total 6 articles about 2,2-dimethylpent-4-enylcarbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2,2-dimethyl-1-amino-pent-4-ene (73604-46-3) + benzyl chloroformate (501-53-1,94274-21-2) → 2,2-dimethylpent-4-enylcarbamic acid benzyl ester (886576-63-2)

Guidance literature:

With potassium carbonate; In 1,4-dioxane; water; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1021/acs.orglett.0c03090

Reference yield: 80.0%

C16H23NO3 (1186589-93-4) → 2,2-dimethylpent-4-enylcarbamic acid benzyl ester (886576-63-2) + C16H21NO2 (1186590-11-3) + C16H21NO2 (1186590-12-4)

Guidance literature:

With iron triflate; In 1,4-dioxane; at 25 ℃; for 2h; Inert atmosphere;

DOI:10.1246/cl.2009.724

Reference yield: 79.0%

C19H27NO5 (1186589-94-5) → 2,2-dimethylpent-4-enylcarbamic acid benzyl ester (886576-63-2) + C16H21NO2 (1186590-11-3) + C16H21NO2 (1186590-12-4)

Guidance literature:

With iron triflate; In 1,4-dioxane; at 25 ℃; for 3h; Inert atmosphere;

DOI:10.1246/cl.2009.724

upstream raw materials:

2,2-dimethyl-1-amino-pent-4-ene

benzyl chloroformate

N-(Benzyloxycarbonyloxy)succinimide

C₁₉H₂₇NO₅

Downstream raw materials:

C₁₆H₂₁NO₃

benzyl 2-(chloromethyl)-4,4-dimethylpyrrolidine-1-carboxylate

benzyl 4,4-dimethyl-2-((N-(phenylsulfonyl)phenylsulfonamido)methyl)-pyrrolidine-1-carboxylate

benzyl 4,4-dimethyl-2-(4-methylbenzyl)-pyrrolidine-1-carboxylate

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