ethyl 2-(6-methoxy-1,2,3,4-tetrahydronaphthalen-1-yl)acetate

Base Information

Chemical Name:ethyl 2-(6-methoxy-1,2,3,4-tetrahydronaphthalen-1-yl)acetate
CAS No.:58491-25-1
Molecular Formula:C₁₅H₂₀O₃
Molecular Weight:248.322
Hs Code.:
Mol file:58491-25-1.mol

Synonyms:6-methoxy-1,2,3,4-tetrahydro-1-naphthyl-acetic acid ethyl ester

Suppliers and Price of ethyl 2-(6-methoxy-1,2,3,4-tetrahydronaphthalen-1-yl)acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of ethyl 2-(6-methoxy-1,2,3,4-tetrahydronaphthalen-1-yl)acetate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Technology Process of ethyl 2-(6-methoxy-1,2,3,4-tetrahydronaphthalen-1-yl)acetate

There total 3 articles about ethyl 2-(6-methoxy-1,2,3,4-tetrahydronaphthalen-1-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.8%

: 25112-94-1,40153-99-9,40154-00-5
(6-methoxy-3,4-dihydro-2H-[1]naphthyliden)-acetic acid ethyl ester

: 58491-25-1
6-methoxy-1,2,3,4-tetrahydro-1-naphthyl-acetic acid ethyl ester

Guidance literature:: With hydrogen; 1% Pd/C; In ethanol; at 20 ℃; for 12h;

Reference yield: 58.5%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 1078-19-9
6-methoxy-3,4-dihydro-1(2H)-naphthalenone

: 58491-25-1
6-methoxy-1,2,3,4-tetrahydro-1-naphthyl-acetic acid ethyl ester

Guidance literature:: diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In toluene; mineral oil; at 0 - 20 ℃; for 0.666667h;

6-methoxy-3,4-dihydro-1(2H)-naphthalenone; In toluene; mineral oil; at 0 ℃; for 14h; Reflux;

With palladium 10% on activated carbon; hydrogen; In ethanol; at 50 ℃; for 5h;
DOI:10.1039/c1ob05299c

Reference yield:

: 1078-19-9
6-methoxy-3,4-dihydro-1(2H)-naphthalenone

: 58491-25-1
6-methoxy-1,2,3,4-tetrahydro-1-naphthyl-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / various solvent(s)

2: hydrogen / Pd/C

With hydrogen; sodium hydride; palladium on activated charcoal; In various solvent(s);
DOI:10.1016/S0968-0896(01)00011-6