3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurepentafluorphenylester

Base Information

Chemical Name:3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurepentafluorphenylester
CAS No.:116527-93-6
Molecular Formula:C₃₉H₃₅F₅N₂O₅
Molecular Weight:706.709
Hs Code.:

Synonyms:3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurepentafluorphenylester

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Chemical Property of 3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurepentafluorphenylester

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Technology Process of 3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurepentafluorphenylester

There total 10 articles about 3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurepentafluorphenylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 116527-84-5
9-(3-Benzyloxy-propyl)-5,8,9,10,11,12-hexahydro-6H-7,12-diaza-cyclonona[a]indene-7,11-dicarboxylic acid 7-benzyl ester

: 116527-93-6
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurepentafluorphenylester

Guidance literature:: With dicyclohexyl-carbodiimide; In ethyl acetate; for 2.5h; Ambient temperature;
DOI:10.1016/S0040-4020(01)86862-9

Reference yield:

: 116527-79-8,116527-80-1
2-(3-benzyloxypropyl)-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indol

: 116527-93-6
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurepentafluorphenylester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) water; / 1.) aceton; 2.) 50 deg C, 1 h

2: 68 percent / HCl / CH₂Cl₂ / 2 h / Ambient temperature

3: 95 percent / water, sodium hydroxide / ethanol / 1.5 h / Heating

4: 67 percent / N,N'-dicyclohexylcarbodiimide / ethyl acetate / 2.5 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; water; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(01)86862-9

Reference yield:

: 116527-78-7,116556-53-7
2-(3-benzyloxypropyl)-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indol-3-on

: 116527-93-6
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurepentafluorphenylester

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / Lithium aluminium hydride / tetrahydrofuran / 1 h / Heating

2: 1.) water; / 1.) aceton; 2.) 50 deg C, 1 h

3: 68 percent / HCl / CH₂Cl₂ / 2 h / Ambient temperature

4: 95 percent / water, sodium hydroxide / ethanol / 1.5 h / Heating

5: 67 percent / N,N'-dicyclohexylcarbodiimide / ethyl acetate / 2.5 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; water; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(01)86862-9