tert-butyl ((2S,3R)-4-(hex-5-en-1-ylamino)-3-hydroxy-1-phenylbutan-2-yl)carbamate

Base Information

• Chemical Name: tert-butyl ((2S,3R)-4-(hex-5-en-1-ylamino)-3-hydroxy-1-phenylbutan-2-yl)carbamate
• CAS No.: 1190426-46-0
• Molecular Formula: C₂₁H₃₄N₂O₃
• Molecular Weight: 362.513

Synonyms:tert-butyl ((2S,3R)-4-(hex-5-en-1-ylamino)-3-hydroxy-1-phenylbutan-2-yl)carbamate

Chemical Property of tert-butyl ((2S,3R)-4-(hex-5-en-1-ylamino)-3-hydroxy-1-phenylbutan-2-yl)carbamate

Chemical Property:

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Technology Process of tert-butyl ((2S,3R)-4-(hex-5-en-1-ylamino)-3-hydroxy-1-phenylbutan-2-yl)carbamate

There total 1 articles about tert-butyl ((2S,3R)-4-(hex-5-en-1-ylamino)-3-hydroxy-1-phenylbutan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

hex-5-en-1-amine (34825-70-2) + (1-oxiranyl-2-phenylethyl)carbamic acid tert-butyl ester (98760-08-8,98818-34-9,98818-35-0,103127-56-6,98737-29-2) → tert-butyl ((2S,3R)-4-(hex-5-en-1-ylamino)-3-hydroxy-1-phenylbutan-2-yl)carbamate (1190426-46-0)

Guidance literature:

In isopropyl alcohol; at 60 ℃; for 4h;

DOI:10.1021/jm900695w

Reference yield: 92.0%

tert-butyl ((2S,3R)-4-(hex-5-en-1-ylamino)-3-hydroxy-1-phenylbutan-2-yl)carbamate (1190426-46-0) + 2-((allyloxy)methyl)-4-methoxybenzenesulfonyl chloride → tert-butyl ((2S,3R)-4-((2-((allyloxy)methyl)-N-(hex-5-en-1-yl)-4-methoxyphenyl)sulfonamido)-3-hydroxy-1-phenylbutan-2-yl)carbamate

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; water; at 23 ℃; for 18h;

Reference yield: 84.0%

2-(hex-5-enyloxy)-4-methoxybenzene-1-sulfonyl chloride (1190427-07-6) + tert-butyl ((2S,3R)-4-(hex-5-en-1-ylamino)-3-hydroxy-1-phenylbutan-2-yl)carbamate (1190426-46-0) → tert-butyl-(2S,3R)-4-(N-(hex-5-enyl)-2-(hex-5-enyloxy)-4-ethoxyphenylsulfonamido)-3-hydroxy-1-phenylbutan-2-ylcarbamate (1190426-47-1)

Guidance literature:

With pyridine; at 23 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jm900695w

upstream raw materials:

hex-5-en-1-amine

(1-oxiranyl-2-phenylethyl)carbamic acid tert-butyl ester

Downstream raw materials:

tert-butyl-(2S,3R)-4-(N-(hex-5-enyl)-2-(hex-5-enyloxy)-4-ethoxyphenylsulfonamido)-3-hydroxy-1-phenylbutan-2-ylcarbamate

tert-butyl-(2S,3R)-4-(N-(hex-5-enyl)-4-methoxy-2-(pent-4-enyloxy)phenylsulfonamido)-3-hydroxy-1-phenylbutan-2-ylcarbamate

tert-butyl-(2S,3R)-4-(2-(but-3-enyloxy)-N-(hex-5-enyl)-4-methoxyphenylsulfonamido)-3-hydroxy-1-phenylbutan-2-ylcarbamate

tert-butyl-(2S,3R)-4-(2-(allyloxy)-N-(hex-5-enyl)-4-methoxyphenylsulfonamido)-3-hydroxy-1-phenylbutan-2-ylcarbamate

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