1-deuteriocyclohex-2-en-1-ol

Base Information

Chemical Name:1-deuteriocyclohex-2-en-1-ol
CAS No.:55282-88-7
Molecular Formula:C₆H₁₀O
Molecular Weight:99.1369
Hs Code.:

Synonyms:1-deuteriocyclohex-2-en-1-ol

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Chemical Property of 1-deuteriocyclohex-2-en-1-ol

Chemical Property:

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Technology Process of 1-deuteriocyclohex-2-en-1-ol

There total 8 articles about 1-deuteriocyclohex-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80642-13-3
C₁₃H₁₁⁽²⁾HN₂O₆

: 55282-88-7
1-deuteriocyclohex-2-en-1-ol

: 73741-72-7
3-deuterio-2-cyclohexen-1-ol

Guidance literature:: With water; N-ethyl-N,N-diisopropylamine; In acetone; at 72.5 ℃; Rate constant; Mechanism; randomization of allylic position;
DOI:10.1021/ja00370a040

Reference yield:

: 5323-87-5
3-Ethoxycyclohex-2-en-1-one

: 55282-88-7
1-deuteriocyclohex-2-en-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: LAD

1.2: Acid hydrolysis

2.1: LiAlH₄; 2-ethylaminopyridine; N-methylephedrine / diethyl ether

3.1: triphenylphosphine; diethyl azodicarboxylate; benzoic acid / tetrahydrofuran / 1 h / 0 °C

3.2: LAH

With 2-(ethylamino)pyridine; lithium aluminium tetrahydride; lithium aluminium deuteride; (-)-N-methylephedrine; triphenylphosphine; benzoic acid; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; 1.1: Reduction / 1.2: Hydrolysis / 2.1: Reduction / 3.1: Mitsunobu reaction / 3.2: Reduction;
DOI:10.1021/jo9615155

Reference yield:

: 75265-49-5
3-deuteriocyclohex-2-en-1-one

: 55282-88-7
1-deuteriocyclohex-2-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: LiAlH₄; 2-ethylaminopyridine; N-methylephedrine / diethyl ether

2.1: triphenylphosphine; diethyl azodicarboxylate; benzoic acid / tetrahydrofuran / 1 h / 0 °C

2.2: LAH

With 2-(ethylamino)pyridine; lithium aluminium tetrahydride; (-)-N-methylephedrine; triphenylphosphine; benzoic acid; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; 1.1: Reduction / 2.1: Mitsunobu reaction / 2.2: Reduction;
DOI:10.1021/jo9615155