6-O-[6'-O-(benzyl)-4'-O-acetyl-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal

Base Information

Chemical Name:6-O-[6'-O-(benzyl)-4'-O-acetyl-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal
CAS No.:1033614-38-8
Molecular Formula:C₂₂H₂₈O₁₀S
Molecular Weight:484.524
Hs Code.:

Synonyms:6-O-[6'-O-(benzyl)-4'-O-acetyl-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal

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Chemical Property of 6-O-[6'-O-(benzyl)-4'-O-acetyl-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal

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Technology Process of 6-O-[6'-O-(benzyl)-4'-O-acetyl-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal

There total 1 articles about 6-O-[6'-O-(benzyl)-4'-O-acetyl-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1033614-36-6
6-O-[6'-O-(benzyl)-4'-O-acetyl-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-3-O-(t-butyldimethylsilyl)-D-glucal

: 1033614-38-8
6-O-[6'-O-(benzyl)-4'-O-acetyl-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol800793f

Reference yield:

: 1033614-31-1
3-O-(t-butyldimethylsilyl)-4-O-mesyl-D-glucal

: 1033614-38-8
6-O-[6'-O-(benzyl)-4'-O-acetyl-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal

: 1033614-40-2
6-O-[6'-O-[6''-O-(benzyl)-4''-O-acetyl-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-3-O-(t-butyldimethylsilyl)-D-glucal

Guidance literature:: 6-O-[6'-O-(benzyl)-4'-O-acetyl-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal; With potassium tert-butylate; In acetonitrile; at 20 ℃; for 0.333333h; Inert atmosphere;

3-O-(t-butyldimethylsilyl)-4-O-mesyl-D-glucal; In acetonitrile; at 20 ℃; for 48h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ol800793f