silver 3-iodo-5-phenylisothiazole-4-carboxylate

Base Information

Chemical Name:silver 3-iodo-5-phenylisothiazole-4-carboxylate
CAS No.:942227-93-2
Molecular Formula:Ag*C₁₀H₅INO₂S
Molecular Weight:437.994
Hs Code.:

Synonyms:silver 3-iodo-5-phenylisothiazole-4-carboxylate

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Chemical Property of silver 3-iodo-5-phenylisothiazole-4-carboxylate

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Technology Process of silver 3-iodo-5-phenylisothiazole-4-carboxylate

There total 1 articles about silver 3-iodo-5-phenylisothiazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 942227-90-9
3-iodo-5-phenylisothiazole-4-carboxylic acid

: silver nitrate

: 942227-93-2
silver 3-iodo-5-phenylisothiazole-4-carboxylate

Guidance literature:: With potassium hydroxide; In water; addn. of a soln. of KOH in water to a stirred mixt. of acid and water, stirring at 20°C, addn. of a soln. of AgNO3 in water; filtration, washing with water, acetone, drying in vac. at 80°C for 12 h;
DOI:10.1039/b702154b

Reference yield: 75.0%

: 942227-93-2
silver 3-iodo-5-phenylisothiazole-4-carboxylate

: 942227-94-3
4-bromo-3-iodo-5-phenylisothiazole

Guidance literature:: With bromine; In tetrachloromethane; at 20 ℃; for 1h;
DOI:10.1039/b702154b

Reference yield:

: 942227-93-2
silver 3-iodo-5-phenylisothiazole-4-carboxylate

: 3920-15-8
3,5-diphenylisothiazole

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / Br₂ / CCl₄ / 1 h / 20 °C

2: K₂CO₃ / Pd(OAc)2 / dimethylformamide / 140 °C

3: 71 percent / (PPh₃)2PdCl₂ / dimethylformamide / 4 h / 100 °C

With bromine; potassium carbonate; bis-triphenylphosphine-palladium(II) chloride; palladium diacetate; In tetrachloromethane; N,N-dimethyl-formamide; 1: Hunsdiercker reaction / 2: Suzuki reaction / 3: Negishi reaction;
DOI:10.1039/b702154b