Technology Process of C33H26N2O9
There total 3 articles about C33H26N2O9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trimethylsilyl trifluoromethanesulfonate;
In
acetonitrile;
at 0 - 85 ℃;
for 20h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tin(II) chloride dihdyrate; lithium iodide trihydrate / 1,2-dimethoxyethane / 1 h / 85 °C
2: dmap; triethylamine / dichloromethane / 4 h / 20 °C
3: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 20 h / 0 - 85 °C
With
dmap; tin(II) chloride dihdyrate; lithium iodide trihydrate; trimethylsilyl trifluoromethanesulfonate; triethylamine;
In
1,2-dimethoxyethane; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dmap; triethylamine / dichloromethane / 4 h / 20 °C
2: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 20 h / 0 - 85 °C
With
dmap; trimethylsilyl trifluoromethanesulfonate; triethylamine;
In
dichloromethane; acetonitrile;