Methyl 4-<4,5-dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoate

Base Information

Chemical Name:Methyl 4-<4,5-dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoate
CAS No.:134248-29-6
Molecular Formula:C₂₁H₁₇N₃O₃
Molecular Weight:359.384
Hs Code.:

Synonyms:Methyl 4-<4,5-dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoate

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Chemical Property of Methyl 4-<4,5-dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoate

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Technology Process of Methyl 4-<4,5-dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoate

There total 1 articles about Methyl 4-<4,5-dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 54753-57-0,70082-68-7,70082-69-8
4-(1'H-indol-3'-ylmethylene)-2-methyl-5(4H)oxazolone

: 619-45-4
4-methoxycarbonyl aniline

: 134248-29-6
Methyl 4-<4,5-dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoate

Guidance literature:: at 140 ℃; for 0.333333h;

Reference yield: 75.0%

: 134248-29-6
Methyl 4-<4,5-dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoate

: 134248-33-2
4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoic acid hydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 8h; Heating;

Reference yield:

: 134248-29-6
Methyl 4-<4,5-dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoate

: 134248-49-0
4-{4-[1-(1H-Indol-3-yl)-meth-(Z)-ylidene]-2-methyl-5-oxo-4,5-dihydro-imidazol-1-yl}-benzoic acid [1-phenyl-1-o-tolylazo-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / 99percent N₂H₄*H₂O / ethanol / 8 h / Heating

2: 75 percent / glacial AcOH / ethanol / 5 h / Heating

3: 1) glacial AcOH, HCl, NaNO₂ 2) pyridine / 1) water, 0-5 deg C 2) r.t., overnight

With pyridine; hydrogenchloride; hydrazine hydrate; acetic acid; sodium nitrite; In ethanol;