3-{4-[({[4-(difluorophosphonomethyl)-3-chlorophenyl]methyl}[(2-methoxyphenyl)sulfonyl]amino)methyl]phenyl}benzenecarbonitrile

Base Information

• Chemical Name: 3-{4-[({[4-(difluorophosphonomethyl)-3-chlorophenyl]methyl}[(2-methoxyphenyl)sulfonyl]amino)methyl]phenyl}benzenecarbonitrile
• CAS No.: 874566-95-7
• Molecular Formula: C₂₉H₂₄ClF₂N₂O₆PS
• Molecular Weight: 633.009

Synonyms:3-{4-[({[4-(difluorophosphonomethyl)-3-chlorophenyl]methyl}[(2-methoxyphenyl)sulfonyl]amino)methyl]phenyl}benzenecarbonitrile

Chemical Property of 3-{4-[({[4-(difluorophosphonomethyl)-3-chlorophenyl]methyl}[(2-methoxyphenyl)sulfonyl]amino)methyl]phenyl}benzenecarbonitrile

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Technology Process of 3-{4-[({[4-(difluorophosphonomethyl)-3-chlorophenyl]methyl}[(2-methoxyphenyl)sulfonyl]amino)methyl]phenyl}benzenecarbonitrile

There total 1 articles about 3-{4-[({[4-(difluorophosphonomethyl)-3-chlorophenyl]methyl}[(2-methoxyphenyl)sulfonyl]amino)methyl]phenyl}benzenecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

3-(4-{[({4-[(diethoxyphosphonyl)difluoromethyl]-3-chlorophenyl}methyl)[(2-methoxyphenyl)sulfonyl]amino]methyl}phenyl)benzenecarbonitrile → 3-{4-[({[4-(difluorophosphonomethyl)-3-chlorophenyl]methyl}[(2-methoxyphenyl)sulfonyl]amino)methyl]phenyl}benzenecarbonitrile (874566-95-7)

Guidance literature:

3-(4-{[({4-[(diethoxyphosphonyl)difluoromethyl]-3-chlorophenyl}methyl)[(2-methoxyphenyl)sulfonyl]amino]methyl}phenyl)benzenecarbonitrile; With trimethylsilyl iodide; In dichloromethane; at -20 ℃; for 1h;

With water; trifluoroacetic acid; In acetonitrile; at 20 ℃;

Reference yield: 73.0%

3-{4-[({[4-(difluorophosphonomethyl)-3-chlorophenyl]methyl}[(2-methoxyphenyl)sulfonyl]amino)methyl]phenyl}benzenecarbonitrile (874566-95-7) → {[4-(difluorophosphonomethyl)-3-chlorophenyl]methyl}[(2-methoxyphenyl)sulfonyl]{[4-(3-(2H-1,2,3,4-tetraazol-5-yl)phenyl)phenyl]methyl}amine

Guidance literature:

With sodium azide; ammonium chloride; In N,N-dimethyl-formamide; at 120 ℃;

Reference yield: 51.0%

3-{4-[({[4-(difluorophosphonomethyl)-3-chlorophenyl]methyl}[(2-methoxyphenyl)sulfonyl]amino)methyl]phenyl}benzenecarbonitrile (874566-95-7) + 1-(isopropoxycarbonyloxy)ethyl chloride (98298-66-9) → [({2-chloro-4-[({[4-(3-cyanophenyl)phenyl]methyl}[(2-methoxyphenyl)sulfonyl]amino)methyl]phenyl}difluoromethyl)(hydroxyphosphoryl)oxy]ethyl(methylethoxy)formate sodium salt

Guidance literature:

3-{4-[({[4-(difluorophosphonomethyl)-3-chlorophenyl]methyl}[(2-methoxyphenyl)sulfonyl]amino)methyl]phenyl}benzenecarbonitrile; 1-(isopropoxycarbonyloxy)ethyl chloride; With caesium carbonate; In acetonitrile; for 18h; Heating / reflux;

With sodium hydrogencarbonate; In methanol; at 20 ℃;

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