(4-fluorophenyl)carbamoyl azide

Base Information

Chemical Name:(4-fluorophenyl)carbamoyl azide
CAS No.:1613145-24-6
Molecular Formula:C₇H₅FN₄O
Molecular Weight:180.141
Hs Code.:

Synonyms:(4-fluorophenyl)carbamoyl azide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-fluorophenyl)carbamoyl azide

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Technology Process of (4-fluorophenyl)carbamoyl azide

There total 4 articles about (4-fluorophenyl)carbamoyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 4648-54-8
trimethylsilylazide

: 63131-29-3
methyl 4-fluorobenzoyl acetate

: 1613145-24-6
(4-fluorophenyl)carbamoyl azide

Guidance literature:: With ammonium cerium (IV) nitrate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen; In ethyl acetate; at 60 ℃; for 36h; under 760.051 Torr; Schlenk technique; Molecular sieve;
DOI:10.1021/ol5014476

Reference yield: 61.0%

: 459-57-4
4-fluorobenzaldehyde

: 1613145-24-6
(4-fluorophenyl)carbamoyl azide

Guidance literature:: With tert.-butylhydroperoxide; trimethylsilylazide; potassium iodide; In ethyl acetate; at 75 ℃; for 36h; Schlenk technique;
DOI:10.1002/cjoc.201600914