{Rh(H)2(3,6-bis(2'-pyridiyl)pyridazine)(triphenylphosphine)2}PF₆*CH₂Cl₂

Base Information

Chemical Name:{Rh(H)2(3,6-bis(2'-pyridiyl)pyridazine)(triphenylphosphine)2}PF₆*CH₂Cl₂
CAS No.:116766-92-8
Molecular Formula:CH₂Cl₂*C₅₀H₄₂N₄P₂Rh*F₆P
Molecular Weight:1093.66
Hs Code.:

{Rh(H)2(3,6-bis(2'-pyridiyl)pyridazine)(triphenylphosphine)2}PF<sub>6</sub>*CH<sub>2</sub>Cl<sub>2</sub>

Synonyms:{Rh(H)2(3,6-bis(2'-pyridiyl)pyridazine)(triphenylphosphine)2}PF₆*CH₂Cl₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {Rh(H)2(3,6-bis(2'-pyridiyl)pyridazine)(triphenylphosphine)2}PF₆*CH₂Cl₂

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Technology Process of {Rh(H)2(3,6-bis(2'-pyridiyl)pyridazine)(triphenylphosphine)2}PF₆*CH₂Cl₂

There total 2 articles about {Rh(H)2(3,6-bis(2'-pyridiyl)pyridazine)(triphenylphosphine)2}PF₆*CH₂Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 82404-88-4,79027-52-4
{Rh(H)2(acetone)2(triphenylphosphine)2}PF₆

: 36901-11-8
3,6-di(pyridin-2'-yl)-s-tetrazine

: 116766-92-8
{Rh(H)2(3,6-bis(2'-pyridiyl)pyridazine)(triphenylphosphine)2}PF₆*CH₂Cl₂

Guidance literature:: In dichloromethane; under N2, stirred; slow addn. of diethyl ether, pptn. recrystd. (CH2Cl2-Et2O); elem. anal.;
DOI:10.1016/S0020-1693(00)83379-4

Reference yield: 68.0%

: {Rh(η4-cod)(3,6-bis(2'-pyridiyl)pyridazine)}PF6

: 116766-92-8
{Rh(H)2(3,6-bis(2'-pyridiyl)pyridazine)(triphenylphosphine)2}PF₆*CH₂Cl₂

Guidance literature:: With triphenylphosphine; hydrogen; In acetone; stored under 3 atm of molecular hydrogen at room temp. for 24 h; pressure released, addn. of diethyl ether, cooled to -20°C, allowed to stand overnight, filtered, dried in vac.; elem. anal.;
DOI:10.1016/S0020-1693(00)83379-4