diisopropyl phenyl(phenylsulfonyl)methylphosphonate

Base Information

Chemical Name:diisopropyl phenyl(phenylsulfonyl)methylphosphonate
CAS No.:428867-18-9
Molecular Formula:C₁₉H₂₅O₅PS
Molecular Weight:396.444
Hs Code.:

Synonyms:diisopropyl phenyl(phenylsulfonyl)methylphosphonate

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Chemical Property of diisopropyl phenyl(phenylsulfonyl)methylphosphonate

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Technology Process of diisopropyl phenyl(phenylsulfonyl)methylphosphonate

There total 2 articles about diisopropyl phenyl(phenylsulfonyl)methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 136052-59-0
(Bromo-phenyl-methyl)-phosphonic acid diisopropyl ester

: 428867-18-9
diisopropyl phenyl(phenylsulfonyl)methylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / dimethylformamide

2: 63 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 24 h

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0111560

Reference yield:

: 108-98-5
thiophenol

: 428867-18-9
diisopropyl phenyl(phenylsulfonyl)methylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / dimethylformamide

2: 63 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 24 h

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0111560

Reference yield: 83.0%

: 428867-18-9
diisopropyl phenyl(phenylsulfonyl)methylphosphonate

: 428867-22-5
diisopropyl [fluoro(phenyl)(phenylsulfonyl)]methylphosphonate

Guidance literature:: diisopropyl phenyl(phenylsulfonyl)methylphosphonate; With potassium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 0.916667h;

With Selectfluor; In tetrahydrofuran; N,N-dimethyl-formamide; for 1.5h; Further stages.;
DOI:10.1021/jo0111560