C₂₅H₁₇ClN₂O₂

Base Information

• Chemical Name: C₂₅H₁₇ClN₂O₂
• CAS No.: 936566-17-5
• Molecular Formula: C₂₅H₁₇ClN₂O₂
• Molecular Weight: 412.875
• Mol file: 936566-17-5.mol

Synonyms:C₂₅H₁₇ClN₂O₂

Chemical Property of C₂₅H₁₇ClN₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₁₇ClN₂O₂

There total 4 articles about C₂₅H₁₇ClN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

C26H19ClN2O2 (936566-30-2) → C25H17ClN2O2 (936566-17-5)

Guidance literature:

C₂₆H₁₉ClN₂O₂; With boron tribromide; In dichloromethane; at 25 ℃; for 2h;

With water; In dichloromethane; for 1h; Further stages.;

DOI:10.1016/j.bmcl.2007.01.043

Reference yield:

(E)-1-(3-chlorophenyl)-3-(4-methoxyphenyl)prop-2-en-1-one → C25H17ClN2O2 (936566-17-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 65 percent / LiOH / tetrahydrofuran / 2 h / 25 °C

2.1: 73 percent / ammonium ferric sulphate dodecahydrate; NH₄OAC; AcOH / 3 h / Heating

3.1: BBr₃ / CH₂Cl₂ / 2 h / 25 °C

3.2: 61 percent / H₂O / CH₂Cl₂ / 1 h

With lithium hydroxide; ammonium iron(III) sulfate dodecahydrate; ammonium acetate; boron tribromide; acetic acid; In tetrahydrofuran; dichloromethane; 1.1: Michael addition;

DOI:10.1016/j.bmcl.2007.01.043

Reference yield:

C26H22ClNO4 (936566-16-4) → C25H17ClN2O2 (936566-17-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 73 percent / ammonium ferric sulphate dodecahydrate; NH₄OAC; AcOH / 3 h / Heating

2.1: BBr₃ / CH₂Cl₂ / 2 h / 25 °C

2.2: 61 percent / H₂O / CH₂Cl₂ / 1 h

With ammonium iron(III) sulfate dodecahydrate; ammonium acetate; boron tribromide; acetic acid; In dichloromethane;

DOI:10.1016/j.bmcl.2007.01.043

upstream raw materials:

C₂₆H₁₉ClN₂O₂

C₂₆H₂₂ClNO₄

1H-[1]benzazepin-2,5(3H,4H)-dione

Downstream raw materials:

C₂₉H₂₄BrClN₂O₂

C₃₇H₂₈ClN₃O₄