benzyl (Z)-7-[(1R,2S,3R,5S)-2-formyl-3-(2-phenylmethoxy)-5-(2-tetrahydropyranyloxy)cyclopentyl]-5-heptanoate

Base Information

Chemical Name:benzyl (Z)-7-[(1R,2S,3R,5S)-2-formyl-3-(2-phenylmethoxy)-5-(2-tetrahydropyranyloxy)cyclopentyl]-5-heptanoate
CAS No.:1236109-35-5
Molecular Formula:C₃₂H₄₀O₆
Molecular Weight:520.666
Hs Code.:

Synonyms:benzyl (Z)-7-[(1R,2S,3R,5S)-2-formyl-3-(2-phenylmethoxy)-5-(2-tetrahydropyranyloxy)cyclopentyl]-5-heptanoate

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Chemical Property of benzyl (Z)-7-[(1R,2S,3R,5S)-2-formyl-3-(2-phenylmethoxy)-5-(2-tetrahydropyranyloxy)cyclopentyl]-5-heptanoate

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Technology Process of benzyl (Z)-7-[(1R,2S,3R,5S)-2-formyl-3-(2-phenylmethoxy)-5-(2-tetrahydropyranyloxy)cyclopentyl]-5-heptanoate

There total 1 articles about benzyl (Z)-7-[(1R,2S,3R,5S)-2-formyl-3-(2-phenylmethoxy)-5-(2-tetrahydropyranyloxy)cyclopentyl]-5-heptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1236109-34-4
benzyl (Z)-7-[(1R,2S,3R,5S)-2-hydroxymethyl-3-(2-phenylmethoxy)-5-(2-tetrahydropyranyloxy)cyclopentyl]-5-heptanoate

: 1236109-35-5
benzyl (Z)-7-[(1R,2S,3R,5S)-2-formyl-3-(2-phenylmethoxy)-5-(2-tetrahydropyranyloxy)cyclopentyl]-5-heptanoate

Guidance literature:: benzyl (Z)-7-[(1R,2S,3R,5S)-2-hydroxymethyl-3-(2-phenylmethoxy)-5-(2-tetrahydropyranyloxy)cyclopentyl]-5-heptanoate; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.75h;

With triethylamine; In dichloromethane; at -78 ℃; for 4h;

Reference yield: 11.0%

: 1236109-35-5
benzyl (Z)-7-[(1R,2S,3R,5S)-2-formyl-3-(2-phenylmethoxy)-5-(2-tetrahydropyranyloxy)cyclopentyl]-5-heptanoate

: 50889-46-8
dimethyl (3,3-difluoro-2-oxoheptyl)-phosphonate

: 1236109-36-6
benzyl (Z)-7-[(1R,2R,3R,5S)-5-(2-tetrahydropyranyloxy)-2-((E)-4,4-difluoro-3-oxo-1-octenyl)-3-(phenylmethoxy)cyclopentyl]heptanoate

Guidance literature:: dimethyl (3,3-difluoro-2-oxoheptyl)-phosphonate; With lithium hydroxide monohydrate; In tert-butyl methyl ether; at 20 - 25 ℃; for 2h;

benzyl (Z)-7-[(1R,2S,3R,5S)-2-formyl-3-(2-phenylmethoxy)-5-(2-tetrahydropyranyloxy)cyclopentyl]-5-heptanoate; In dichloromethane; tert-butyl methyl ether; water; for 72h; Product distribution / selectivity; Reflux;