N-cyano-N'-(6-(2-difluoromethoxy-5-chlorophenoxy)hexyl)-N-(4-pyridyl) guanidine

Base Information

Chemical Name:N-cyano-N'-(6-(2-difluoromethoxy-5-chlorophenoxy)hexyl)-N-(4-pyridyl) guanidine
CAS No.:1325728-75-3
Molecular Formula:C₂₀H₂₂ClF₂N₅O₂
Molecular Weight:437.877
Hs Code.:

Synonyms:N-cyano-N'-(6-(2-difluoromethoxy-5-chlorophenoxy)hexyl)-N-(4-pyridyl) guanidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-cyano-N'-(6-(2-difluoromethoxy-5-chlorophenoxy)hexyl)-N-(4-pyridyl) guanidine

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Technology Process of N-cyano-N'-(6-(2-difluoromethoxy-5-chlorophenoxy)hexyl)-N-(4-pyridyl) guanidine

There total 5 articles about N-cyano-N'-(6-(2-difluoromethoxy-5-chlorophenoxy)hexyl)-N-(4-pyridyl) guanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.5%

: 1325728-96-8
6-(5-chloro-2-difluoromethoxy-phenoxy)hexyl-1-amine

: 167552-44-5
1-cyano-2-phenyl-3-(pyrid-4-yl)-isourea

: 1325728-75-3
N-cyano-N'-(6-(2-difluoromethoxy-5-chlorophenoxy)hexyl)-N-(4-pyridyl) guanidine

Guidance literature:: With triethylamine; In ethanol; at 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: tert-butyl 6-(5-chloro-2-difluoromethoxy-phenoxy)hexyl carbamate

: 1325728-75-3
N-cyano-N'-(6-(2-difluoromethoxy-5-chlorophenoxy)hexyl)-N-(4-pyridyl) guanidine

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 3 h / Cooling with ice; Inert atmosphere

2: triethylamine / ethanol / 2 h / 20 °C / Inert atmosphere

With triethylamine; trifluoroacetic acid; In ethanol; dichloromethane;

Reference yield:

: 2138-22-9
4-chloro-1,2-benzenediol

: 1325728-75-3
N-cyano-N'-(6-(2-difluoromethoxy-5-chlorophenoxy)hexyl)-N-(4-pyridyl) guanidine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / N,N-dimethyl-formamide / 1 h / 125 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / Cooling with ice; Inert atmosphere

2.2: 20 °C / Cooling with ice; Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 3 h / Cooling with ice; Inert atmosphere

4.1: triethylamine / ethanol / 2 h / 20 °C / Inert atmosphere

With sodium hydride; triethylamine; trifluoroacetic acid; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;