5-chloro-2-[diisopropyl(pyrimidin-2-yl)silyl]-1,3-phenylene bis(2,2-dimethylpropanoate)

Base Information

Chemical Name:5-chloro-2-[diisopropyl(pyrimidin-2-yl)silyl]-1,3-phenylene bis(2,2-dimethylpropanoate)
CAS No.:1369625-47-7
Molecular Formula:C₂₆H₃₇ClN₂O₄Si
Molecular Weight:505.129
Hs Code.:

Synonyms:5-chloro-2-[diisopropyl(pyrimidin-2-yl)silyl]-1,3-phenylene bis(2,2-dimethylpropanoate)

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Chemical Property of 5-chloro-2-[diisopropyl(pyrimidin-2-yl)silyl]-1,3-phenylene bis(2,2-dimethylpropanoate)

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Technology Process of 5-chloro-2-[diisopropyl(pyrimidin-2-yl)silyl]-1,3-phenylene bis(2,2-dimethylpropanoate)

There total 2 articles about 5-chloro-2-[diisopropyl(pyrimidin-2-yl)silyl]-1,3-phenylene bis(2,2-dimethylpropanoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1369625-63-7
2-((4-chlorophenyl)diisopropylsilyl)pyrimidine

: 57357-20-7
bis(tertbutylcarbonyloxy)iodobenzene

: 1369625-47-7
5-chloro-2-[diisopropyl(pyrimidin-2-yl)silyl]-1,3-phenylene bis(2,2-dimethylpropanoate)

Guidance literature:: With lithium acetate; palladium diacetate; In 1,2-dichloro-ethane; at 80 ℃; for 43h; Inert atmosphere;
DOI:10.1021/ja3010545

Reference yield:

: 1369625-74-0
2-(diisopropylsilyl)pyrimidine

: 1369625-47-7
5-chloro-2-[diisopropyl(pyrimidin-2-yl)silyl]-1,3-phenylene bis(2,2-dimethylpropanoate)

Guidance literature:: Multi-step reaction with 2 steps

1: potassium phosphate; dirhodium tetraacetate / 1,4-dioxane / 6 h / 100 °C / Inert atmosphere

2: lithium acetate; palladium diacetate / 1,2-dichloro-ethane / 43 h / 80 °C / Inert atmosphere

With dirhodium tetraacetate; potassium phosphate; lithium acetate; palladium diacetate; In 1,4-dioxane; 1,2-dichloro-ethane;
DOI:10.1021/ja3010545