C₂₇H₃₇N₂O₈P

Base Information

Chemical Name:C₂₇H₃₇N₂O₈P
CAS No.:1422516-59-3
Molecular Formula:C₂₇H₃₇N₂O₈P
Molecular Weight:548.573
Hs Code.:

C<sub>27</sub>H<sub>37</sub>N<sub>2</sub>O<sub>8</sub>P

Synonyms:C₂₇H₃₇N₂O₈P

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Chemical Property of C₂₇H₃₇N₂O₈P

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Technology Process of C₂₇H₃₇N₂O₈P

There total 7 articles about C₂₇H₃₇N₂O₈P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1422516-55-9
Boc-Leu-Glu(OBzl)^P(OPh)₂

: 1422516-59-3
C₂₇H₃₇N₂O₈P

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 6h;
DOI:10.1016/j.bmcl.2012.12.074

Reference yield:

: 77393-49-8
diphenyl [(([(phenylmethyl)oxy]carbonyl)amino)methyl]phosphonate

: 1422516-59-3
C₂₇H₃₇N₂O₈P

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid; hydrogen bromide / 2 h / 20 °C

2.1: dichloromethane / 24 h / 20 °C

3.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

3.2: 3 h / Inert atmosphere

4.1: hydrogenchloride / diethyl ether / 24 h / 20 °C

5.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / acetonitrile / 12 h / 20 °C

6.1: hydrogen; palladium 10% on activated carbon / methanol / 6 h / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen bromide; hydrogen; potassium hexamethylsilazane; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2012.12.074

Reference yield:

: 77393-50-1
diphenyl (aminomethyl)phosphonate hydrobromide

: 1422516-59-3
C₂₇H₃₇N₂O₈P

Guidance literature:: Multi-step reaction with 5 steps

1.1: dichloromethane / 24 h / 20 °C

2.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 3 h / Inert atmosphere

3.1: hydrogenchloride / diethyl ether / 24 h / 20 °C

4.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / acetonitrile / 12 h / 20 °C

5.1: hydrogen; palladium 10% on activated carbon / methanol / 6 h / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; potassium hexamethylsilazane; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2012.12.074