1-(3'-azido-2'-O-acetyl-5'-O-benzoyl-3'-deoxy-β-D-ribofuranosyl)-N⁴-benzoylcytosine

Base Information

• Chemical Name: 1-(3'-azido-2'-O-acetyl-5'-O-benzoyl-3'-deoxy-β-D-ribofuranosyl)-N⁴-benzoylcytosine
• CAS No.: 917239-18-0
• Molecular Formula: C₂₅H₂₂N₆O₇
• Molecular Weight: 518.486

Synonyms:1-(3'-azido-2'-O-acetyl-5'-O-benzoyl-3'-deoxy-β-D-ribofuranosyl)-N⁴-benzoylcytosine

Chemical Property of 1-(3'-azido-2'-O-acetyl-5'-O-benzoyl-3'-deoxy-β-D-ribofuranosyl)-N⁴-benzoylcytosine

Chemical Property:

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Technology Process of 1-(3'-azido-2'-O-acetyl-5'-O-benzoyl-3'-deoxy-β-D-ribofuranosyl)-N⁴-benzoylcytosine

There total 1 articles about 1-(3'-azido-2'-O-acetyl-5'-O-benzoyl-3'-deoxy-β-D-ribofuranosyl)-N⁴-benzoylcytosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

3-azido-1,2-bis-O-acetyl-5-O-benzoyl-3-deoxy-D-ribofuranose + 4-N-benzoylcytosine (26661-13-2) → 1-(3'-azido-2'-O-acetyl-5'-O-benzoyl-3'-deoxy-β-D-ribofuranosyl)-N4-benzoylcytosine (917239-18-0)

Guidance literature:

3-azido-1,2-bis-O-acetyl-5-O-benzoyl-3-deoxy-D-ribofuranose; 4-N-benzoylcytosine; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; at 50 - 60 ℃; for 1h;

With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 65 - 70 ℃; for 4h;

DOI:10.1080/15257770500267170

Reference yield: 75.0%

1-(3'-azido-2'-O-acetyl-5'-O-benzoyl-3'-deoxy-β-D-ribofuranosyl)-N4-benzoylcytosine (917239-18-0) → 1-(3'-azido-3'-deoxy-β-D-ribofuranosyl)cytosine (60786-48-3)

Guidance literature:

With ammonia; In methanol; at 20 ℃; for 16h;

DOI:10.1080/15257770500267170

Reference yield: 71.0%

1-(3'-azido-2'-O-acetyl-5'-O-benzoyl-3'-deoxy-β-D-ribofuranosyl)-N4-benzoylcytosine (917239-18-0) → 1-(3'-azido-5'-O-benzoyl-3'-deoxy-β-D-ribofuranosyl)cytosine

Guidance literature:

With pyridine; hydrazine hydrate; acetic acid; at 20 ℃; for 24h;

DOI:10.1080/15257770500267170

upstream raw materials:

4-N-benzoylcytosine

Downstream raw materials:

1-(3'-azido-3'-deoxy-β-D-ribofuranosyl)cytosine

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