(+)-N-Cbz-galbulimima alkaloid 13

Base Information

Chemical Name:(+)-N-Cbz-galbulimima alkaloid 13
CAS No.:901121-97-9
Molecular Formula:C₂₈H₃₅NO₄
Molecular Weight:449.59
Hs Code.:

Synonyms:(+)-N-Cbz-galbulimima alkaloid 13

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Chemical Property of (+)-N-Cbz-galbulimima alkaloid 13

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Technology Process of (+)-N-Cbz-galbulimima alkaloid 13

There total 15 articles about (+)-N-Cbz-galbulimima alkaloid 13 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 929119-04-0
C₂₈H₃₇NO₄

: 901121-97-9
(+)-N-Cbz-galbulimima alkaloid 13

Guidance literature:: With toluene-4-sulfonic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; benzene; at 65 ℃; for 6h;
DOI:10.1021/ja0684996

Reference yield: 67.0%

: 901121-94-6
C₃₁H₄₀N₂O₅

: 901121-97-9
(+)-N-Cbz-galbulimima alkaloid 13

Guidance literature:: With toluene-4-sulfonic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethylsulfoxide-d6; benzene-d6; at 65 ℃; for 10h;
DOI:10.1021/ja0626180

Reference yield:

: C₂₀H₃₃NO₂

: 901121-97-9
(+)-N-Cbz-galbulimima alkaloid 13

Guidance literature:: Multi-step reaction with 3 steps

1: Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂ / 0.5 h

2: 6 mg / aq. Na₂CO₃ / CH₂Cl₂ / 2.5 h / 0 - 20 °C

3: 90 percent / IBX; p-toluenesulfonic acid / dimethylsulfoxide; benzene / 6 h / 65 °C

With sodium hydrogencarbonate; sodium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dichloromethane; dimethyl sulfoxide; benzene;
DOI:10.1021/ja0684996