4,4,5,5-tetramethyl-2-((1E,3E)-2-methyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)buta-1,3-dien-1-yl)-1,3,2-dioxaborolane

Base Information

Chemical Name:4,4,5,5-tetramethyl-2-((1E,3E)-2-methyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)buta-1,3-dien-1-yl)-1,3,2-dioxaborolane
CAS No.:1440508-12-2
Molecular Formula:C₂₀H₃₃BO₂
Molecular Weight:316.292
Hs Code.:

Synonyms:4,4,5,5-tetramethyl-2-((1E,3E)-2-methyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)buta-1,3-dien-1-yl)-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4,5,5-tetramethyl-2-((1E,3E)-2-methyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)buta-1,3-dien-1-yl)-1,3,2-dioxaborolane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4,4,5,5-tetramethyl-2-((1E,3E)-2-methyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)buta-1,3-dien-1-yl)-1,3,2-dioxaborolane

There total 1 articles about 4,4,5,5-tetramethyl-2-((1E,3E)-2-methyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)buta-1,3-dien-1-yl)-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 550364-43-7
((1E,3E)-2-methyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)buta-1,3-dien-1-yl)boronic acid

: 1440508-12-2
4,4,5,5-tetramethyl-2-((1E,3E)-2-methyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)buta-1,3-dien-1-yl)-1,3,2-dioxaborolane

Guidance literature:: at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja402891m

Reference yield: 54.0%

: 1440508-11-1
(+)-(2R,3R)-2,3-dihydroxy-3-methylpent-4-en-1-yl 4-methoxybenzoate

: 1440508-12-2
4,4,5,5-tetramethyl-2-((1E,3E)-2-methyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)buta-1,3-dien-1-yl)-1,3,2-dioxaborolane

: (+)-(2R,3R,4E,6E,8E)-2,3-dihydroxy-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-4,6,8-trienyl 4-methoxybenzoate

Guidance literature:: With [1,2-bis-(phenylsulfinyl)ethane]palladium(II) acetate; 2,6-dimethyl-1,4-benzoquinone; oxygen; acetic acid; In N,N-dimethyl-formamide; at 40 ℃; for 72h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ja402891m