1-[3,5-bis(2-{4-[2-ethylhexyloxy]phenyl}acetylen-1-yl)phenyl]-2-bromoacetylene

Base Information

Chemical Name:1-[3,5-bis(2-{4-[2-ethylhexyloxy]phenyl}acetylen-1-yl)phenyl]-2-bromoacetylene
CAS No.:1170669-77-8
Molecular Formula:C₄₀H₄₅BrO₂
Molecular Weight:637.7
Hs Code.:

Synonyms:1-[3,5-bis(2-{4-[2-ethylhexyloxy]phenyl}acetylen-1-yl)phenyl]-2-bromoacetylene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[3,5-bis(2-{4-[2-ethylhexyloxy]phenyl}acetylen-1-yl)phenyl]-2-bromoacetylene

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Technology Process of 1-[3,5-bis(2-{4-[2-ethylhexyloxy]phenyl}acetylen-1-yl)phenyl]-2-bromoacetylene

There total 1 articles about 1-[3,5-bis(2-{4-[2-ethylhexyloxy]phenyl}acetylen-1-yl)phenyl]-2-bromoacetylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1170669-76-7
1-[3,5-bis(2-{4-[2-ethylhexyloxy]phenyl}acetylen-1-yl)phenyl]-2,2-dibromovinylene

: 1170669-77-8
1-[3,5-bis(2-{4-[2-ethylhexyloxy]phenyl}acetylen-1-yl)phenyl]-2-bromoacetylene

Guidance literature:: With sodium t-butanolate; In toluene; at 50 ℃; for 15h; Inert atmosphere;
DOI:10.1039/b820235d

Reference yield: 93.0%

: 1170669-77-8
1-[3,5-bis(2-{4-[2-ethylhexyloxy]phenyl}acetylen-1-yl)phenyl]-2-bromoacetylene

: 1170669-78-9
[3,5-bis(2-{4-[2-ethylhexyloxy]phenyl}acetylen-1-yl)phenyl]acetylene

Guidance literature:: 1-[3,5-bis(2-{4-[2-ethylhexyloxy]phenyl}acetylen-1-yl)phenyl]-2-bromoacetylene; With tert.-butyl lithium; In tetrahydrofuran; diethyl ether; at -78 ℃; Inert atmosphere;

With water; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1039/b820235d