5-((S)-3-((4S,5S)-5-ethyl-2,2-dimethyl-1,3-dioxolan-4-yl)pentylsulfonyl)-1-phenyl-1H-tetrazole

Base Information

Chemical Name:5-((S)-3-((4S,5S)-5-ethyl-2,2-dimethyl-1,3-dioxolan-4-yl)pentylsulfonyl)-1-phenyl-1H-tetrazole
CAS No.:460076-97-5
Molecular Formula:C₁₉H₂₈N₄O₄S
Molecular Weight:408.522
Hs Code.:

Synonyms:5-((S)-3-((4S,5S)-5-ethyl-2,2-dimethyl-1,3-dioxolan-4-yl)pentylsulfonyl)-1-phenyl-1H-tetrazole

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Chemical Property of 5-((S)-3-((4S,5S)-5-ethyl-2,2-dimethyl-1,3-dioxolan-4-yl)pentylsulfonyl)-1-phenyl-1H-tetrazole

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Technology Process of 5-((S)-3-((4S,5S)-5-ethyl-2,2-dimethyl-1,3-dioxolan-4-yl)pentylsulfonyl)-1-phenyl-1H-tetrazole

There total 7 articles about 5-((S)-3-((4S,5S)-5-ethyl-2,2-dimethyl-1,3-dioxolan-4-yl)pentylsulfonyl)-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 5-[(S)-3-((4S,5S)-5-Ethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-pentylsulfanyl]-1-phenyl-1H-tetrazole

: 460076-97-5
5-((S)-3-((4S,5S)-5-ethyl-2,2-dimethyl-1,3-dioxolan-4-yl)pentylsulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; In ethanol; water; at 0 - 20 ℃;
DOI:10.1021/jo101224w

Reference yield:

: 1576-87-0
trans-2-pentenal

: 460076-97-5
5-((S)-3-((4S,5S)-5-ethyl-2,2-dimethyl-1,3-dioxolan-4-yl)pentylsulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / diethyl ether

2: 68 percent / H⁺ / Heating

3: AD mix-α; CH3SO2NH2 / 48 h

4: LAH / diethyl ether

5: PTSA

6: DEAD; PPh₃

7: aq. H₂O₂ / (NH₄)6Mo₇O₂₄

With AD-mix-α; lithium aluminium tetrahydride; methanesulfonamide; dihydrogen peroxide; hydrogen cation; toluene-4-sulfonic acid; triphenylphosphine; diethylazodicarboxylate; ammonium heptamolybdate; In diethyl ether; 3: Claisen rearrangement Johnson variant;
DOI:10.1021/ja026728s

Reference yield:

: 35077-65-7
(+/-)-(E)-hept-4-en-3-ol

: 460076-97-5
5-((S)-3-((4S,5S)-5-ethyl-2,2-dimethyl-1,3-dioxolan-4-yl)pentylsulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 6 steps

1: 68 percent / H⁺ / Heating

2: AD mix-α; CH3SO2NH2 / 48 h

3: LAH / diethyl ether

4: PTSA

5: DEAD; PPh₃

6: aq. H₂O₂ / (NH₄)6Mo₇O₂₄

With AD-mix-α; lithium aluminium tetrahydride; methanesulfonamide; dihydrogen peroxide; hydrogen cation; toluene-4-sulfonic acid; triphenylphosphine; diethylazodicarboxylate; ammonium heptamolybdate; In diethyl ether; 2: Claisen rearrangement Johnson variant;
DOI:10.1021/ja026728s