1-({[(3-(tert-butyldiphenylsilanyl)prop-2-ynyl)oxy]dithio}oxy)-3-(tert-butyldiphenylsilanyl)prop-2-yne

Base Information

Chemical Name:1-({[(3-(tert-butyldiphenylsilanyl)prop-2-ynyl)oxy]dithio}oxy)-3-(tert-butyldiphenylsilanyl)prop-2-yne
CAS No.:1319722-53-6
Molecular Formula:C₃₈H₄₂O₂S₂Si₂
Molecular Weight:651.053
Hs Code.:

Synonyms:1-({[(3-(tert-butyldiphenylsilanyl)prop-2-ynyl)oxy]dithio}oxy)-3-(tert-butyldiphenylsilanyl)prop-2-yne

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Chemical Property of 1-({[(3-(tert-butyldiphenylsilanyl)prop-2-ynyl)oxy]dithio}oxy)-3-(tert-butyldiphenylsilanyl)prop-2-yne

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Technology Process of 1-({[(3-(tert-butyldiphenylsilanyl)prop-2-ynyl)oxy]dithio}oxy)-3-(tert-butyldiphenylsilanyl)prop-2-yne

There total 3 articles about 1-({[(3-(tert-butyldiphenylsilanyl)prop-2-ynyl)oxy]dithio}oxy)-3-(tert-butyldiphenylsilanyl)prop-2-yne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 126741-70-6
1-<(1',1'-dimethylethyl)diphenylsilyl>prop-1-yn-3-ol

: 1319722-53-6
1-({[(3-(tert-butyldiphenylsilanyl)prop-2-ynyl)oxy]dithio}oxy)-3-(tert-butyldiphenylsilanyl)prop-2-yne

Guidance literature:: With disulfur dichloride; triethylamine; In diethyl ether; at 0 ℃; for 1h;
DOI:10.1055/s-0030-1260024

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1319722-53-6
1-({[(3-(tert-butyldiphenylsilanyl)prop-2-ynyl)oxy]dithio}oxy)-3-(tert-butyldiphenylsilanyl)prop-2-yne

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 2 h / -78 - 20 °C

2: CSA / ethanol / Reflux

3: disulfur dichloride; triethylamine / diethyl ether / 1 h / 0 °C

With disulfur dichloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; triethylamine; In tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1055/s-0030-1260024

Reference yield:

: tert-Butyl-diphenyl-[3-(tetrahydro-pyran-2-yloxy)-prop-1-ynyl]-silane

: 1319722-53-6
1-({[(3-(tert-butyldiphenylsilanyl)prop-2-ynyl)oxy]dithio}oxy)-3-(tert-butyldiphenylsilanyl)prop-2-yne

Guidance literature:: Multi-step reaction with 2 steps

1: CSA / ethanol / Reflux

2: disulfur dichloride; triethylamine / diethyl ether / 1 h / 0 °C

With disulfur dichloride; triethylamine; In diethyl ether; ethanol;
DOI:10.1055/s-0030-1260024