1(3)-O-(β-benzoylpropionyl)-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3(1),4(6),5,6(4)-tetra-O-acetyl-sn-myoinositol

Base Information

• Chemical Name: 1(3)-O-(β-benzoylpropionyl)-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3(1),4(6),5,6(4)-tetra-O-acetyl-sn-myoinositol
• CAS No.: 80065-86-7
• Molecular Formula: C₃₈H₄₆O₂₁
• Molecular Weight: 838.771

Synonyms:1(3)-O-(β-benzoylpropionyl)-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3(1),4(6),5,6(4)-tetra-O-acetyl-sn-myoinositol

Chemical Property of 1(3)-O-(β-benzoylpropionyl)-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3(1),4(6),5,6(4)-tetra-O-acetyl-sn-myoinositol

Chemical Property:

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Technology Process of 1(3)-O-(β-benzoylpropionyl)-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3(1),4(6),5,6(4)-tetra-O-acetyl-sn-myoinositol

There total 4 articles about 1(3)-O-(β-benzoylpropionyl)-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3(1),4(6),5,6(4)-tetra-O-acetyl-sn-myoinositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

1(3)-O-β-benzoylpropionyl-3(1),4(6),5,6(4)-tetra-O-acetyl-sn-myoinositol (80065-84-5) + D-mannose ethyl orthoacetate (3254-15-7,3254-17-9,19189-53-8,28140-37-6,29907-27-5,38081-38-8,63950-42-5,65336-76-7,70749-16-5,92937-14-9,93601-64-0,93601-65-1,127910-77-4) → 1(3)-O-(β-benzoylpropionyl)-2-O-(2,3,4,6-tetra-O-acetyl-β-D-mannopyranosyl)-3(1),4(6),5,6(4)-tetra-O-acetyl-sn-myoinositol (80065-86-7) + 1(3)-O-(β-benzoylpropionyl)-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3(1),4(6),5,6(4)-tetra-O-acetyl-sn-myoinositol (80065-86-7)

Guidance literature:

Reference yield: 5.0%

1(3)-O-β-benzoylpropionyl-3(1),4(6),5,6(4)-tetra-O-acetyl-sn-myoinositol (80065-84-5) + D-mannose ethyl orthoacetate (3254-15-7,3254-17-9,19189-53-8,28140-37-6,29907-27-5,38081-38-8,63950-42-5,65336-76-7,70749-16-5,92937-14-9,93601-64-0,93601-65-1,127910-77-4) → 1(3)-O-(β-benzoylpropionyl)-2-O-(2,3,4,6-tetra-O-acetyl-β-D-mannopyranosyl)-3(1),4(6),5,6(4)-tetra-O-acetyl-sn-myoinositol (80065-86-7) + 1(3)-O-(β-benzoylpropionyl)-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3(1),4(6),5,6(4)-tetra-O-acetyl-sn-myoinositol (80065-86-7)

Guidance literature:

Reference yield:

1(3),4(6),5,6(4)-tetra-O-acetyl-sn-myo-inositol (13462-79-8,80953-32-8,90366-30-6,108032-48-0,113973-54-9,113973-61-8) → 1(3)-O-(β-benzoylpropionyl)-2-O-(2,3,4,6-tetra-O-acetyl-β-D-mannopyranosyl)-3(1),4(6),5,6(4)-tetra-O-acetyl-sn-myoinositol (80065-86-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 88.6 percent / dicyclohexylcarbodiimide

With dicyclohexyl-carbodiimide;

upstream raw materials:

1(3)-O-β-benzoylpropionyl-3(1),4(6),5,6(4)-tetra-O-acetyl-sn-myoinositol

D-mannose ethyl orthoacetate

1⁽³⁾,4⁽⁶⁾,5,6⁽⁴⁾-tetra-O-acetyl-sn-myo-inositol

Downstream raw materials:

2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-1(3),4(6),5,6(4)-tetra-O-acetyl-sn-myo-inositol

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