(+)-(3S,4R)-3-<<2(S)-<(methoxymethoxy)methyl>pyrrolidinyl>carbonyl>-4-phenylcyclohex-1-ene

Base Information

Chemical Name:(+)-(3S,4R)-3-<<2(S)-<(methoxymethoxy)methyl>pyrrolidinyl>carbonyl>-4-phenylcyclohex-1-ene
CAS No.:113133-25-8
Molecular Formula:C₂₀H₂₇NO₃
Molecular Weight:329.439
Hs Code.:

Synonyms:(+)-(3S,4R)-3-<<2(S)-<(methoxymethoxy)methyl>pyrrolidinyl>carbonyl>-4-phenylcyclohex-1-ene

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Chemical Property of (+)-(3S,4R)-3-<<2(S)-<(methoxymethoxy)methyl>pyrrolidinyl>carbonyl>-4-phenylcyclohex-1-ene

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Technology Process of (+)-(3S,4R)-3-<<2(S)-<(methoxymethoxy)methyl>pyrrolidinyl>carbonyl>-4-phenylcyclohex-1-ene

There total 5 articles about (+)-(3S,4R)-3-<<2(S)-<(methoxymethoxy)methyl>pyrrolidinyl>carbonyl>-4-phenylcyclohex-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 113133-24-7
1-<<2(S)-pyrrolidinyl>carbonyl>-2-phenylbenzene

: 113215-81-9
(-)-(3R,4S)-3-<<2(S)-<(methoxymethoxy)methyl>pyrrolidinyl>carbonyl>-4-phenylcycloh-1-ene

: 113133-25-8
(+)-(3S,4R)-3-<<2(S)-<(methoxymethoxy)methyl>pyrrolidinyl>carbonyl>-4-phenylcyclohex-1-ene

: 113215-82-0
(-)-(1R,2S)-1-<<2(S)-<(methoxymethoxy)methyl>pyrrolidinyl>carbonyl>-2-phenylcyclohexane

Guidance literature:: With ammonia; tert-butyl alcohol; In tetrahydrofuran; at -78 ℃; for 0.166667h; Yield given. Yields of byproduct given;
DOI:10.1021/jo00246a012

Reference yield:

: 14002-52-9
o-phenylbenzoyl chloride

: 113133-25-8
(+)-(3S,4R)-3-<<2(S)-<(methoxymethoxy)methyl>pyrrolidinyl>carbonyl>-4-phenylcyclohex-1-ene

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 2 h / -20 °C

2: 92 percent / diisopropylethylamine / CH₂Cl₂ / 12 h / Ambient temperature

3: K, NH₃, t-BuOH / tetrahydrofuran / 0.75 h / -78 °C

With ammonia; N-ethyl-N,N-diisopropylamine; tert-butyl alcohol; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00246a012

Reference yield:

: 113133-13-4
1-<<2(S)-(hydroxymethyl)pyrrolidinyl>carbonyl>-2-phenylbenzene

: 113133-25-8
(+)-(3S,4R)-3-<<2(S)-<(methoxymethoxy)methyl>pyrrolidinyl>carbonyl>-4-phenylcyclohex-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / diisopropylethylamine / CH₂Cl₂ / 12 h / Ambient temperature

2: K, NH₃, t-BuOH / tetrahydrofuran / 0.75 h / -78 °C

With ammonia; N-ethyl-N,N-diisopropylamine; tert-butyl alcohol; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00246a012