(Z)-N-((E)-3-(phenylthiomethylene) tetrahydro-2H-thiopyran-2-ylidene) aniline

Base Information

Chemical Name:(Z)-N-((E)-3-(phenylthiomethylene) tetrahydro-2H-thiopyran-2-ylidene) aniline
CAS No.:1231172-83-0
Molecular Formula:C₁₈H₁₇NS₂
Molecular Weight:311.472
Hs Code.:

Synonyms:(Z)-N-((E)-3-(phenylthiomethylene) tetrahydro-2H-thiopyran-2-ylidene) aniline

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Chemical Property of (Z)-N-((E)-3-(phenylthiomethylene) tetrahydro-2H-thiopyran-2-ylidene) aniline

Chemical Property:

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Technology Process of (Z)-N-((E)-3-(phenylthiomethylene) tetrahydro-2H-thiopyran-2-ylidene) aniline

There total 6 articles about (Z)-N-((E)-3-(phenylthiomethylene) tetrahydro-2H-thiopyran-2-ylidene) aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1231177-55-1
(E)-5-hydroxy-N-phenyl-2-(phenylthiomethylene)pentanethioamide

: 1231172-83-0
(Z)-N-((E)-3-(phenylthiomethylene) tetrahydro-2H-thiopyran-2-ylidene) aniline

Guidance literature:: With methanesulfonyl chloride; triethylamine; sodium iodide; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 151647-02-8
(E)-(2-oxo-2H-pyran-3(4H, 5H, 6H)-ylidene)methyl methanesulfonate

: 1231172-83-0
(Z)-N-((E)-3-(phenylthiomethylene) tetrahydro-2H-thiopyran-2-ylidene) aniline

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 0 °C

1.2: 0.5 h

2.1: diethylaluminium chloride / dichloromethane; hexane / 0.08 h / 20 °C

2.2: 2 h / 20 °C

2.3: 0.5 h / 20 °C

3.1: 1H-imidazole / dichloromethane / 2 h / 20 °C

4.1: tetrahydrofuran / Reflux

5.1: tetrabutyl-ammonium chloride / tetrahydrofuran / 0.5 h / 20 °C

6.1: triethylamine; methanesulfonyl chloride / sodium iodide / dichloromethane / 3 h / 20 °C

With 1H-imidazole; tetrabutyl-ammonium chloride; diethylaluminium chloride; sodium hydride; methanesulfonyl chloride; triethylamine; sodium iodide; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1231177-50-6
(E)-3-(phenylthiomethylene)tetrahydro-2H-pyran-2-one

: 1231172-83-0
(Z)-N-((E)-3-(phenylthiomethylene) tetrahydro-2H-thiopyran-2-ylidene) aniline

Guidance literature:: Multi-step reaction with 5 steps

1.1: diethylaluminium chloride / dichloromethane; hexane / 0.08 h / 20 °C

1.2: 2 h / 20 °C

1.3: 0.5 h / 20 °C

2.1: 1H-imidazole / dichloromethane / 2 h / 20 °C

3.1: tetrahydrofuran / Reflux

4.1: tetrabutyl-ammonium chloride / tetrahydrofuran / 0.5 h / 20 °C

5.1: triethylamine; methanesulfonyl chloride / sodium iodide / dichloromethane / 3 h / 20 °C

With 1H-imidazole; tetrabutyl-ammonium chloride; diethylaluminium chloride; methanesulfonyl chloride; triethylamine; sodium iodide; In tetrahydrofuran; hexane; dichloromethane;