3-trifluoroacetamidopropyl (2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:3-trifluoroacetamidopropyl (2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside
CAS No.:497869-66-6
Molecular Formula:C₇₄H₈₃F₃N₂O₁₆
Molecular Weight:1313.47
Hs Code.:

3-trifluoroacetamidopropyl (2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Synonyms:3-trifluoroacetamidopropyl (2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

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Chemical Property of 3-trifluoroacetamidopropyl (2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Chemical Property:

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Technology Process of 3-trifluoroacetamidopropyl (2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

There total 5 articles about 3-trifluoroacetamidopropyl (2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78008-15-8
N-(3-hydroxypropyl)trifluoroacetamide

: 497869-66-6
3-trifluoroacetamidopropyl (2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 69 percent / BF₃*Et₂O / diethyl ether / 20 °C

2.1: 100 percent / aq. CF₃COOH / CH₂Cl₂ / 0.5 h / 0 °C

3.1: Bu₂SnO / toluene / 3 h / Heating

3.2: tetrabutylammonium iodide / toluene / Heating

With boron trifluoride diethyl etherate; di(n-butyl)tin oxide; trifluoroacetic acid; In diethyl ether; dichloromethane; toluene;
DOI:10.1039/b205684d

Reference yield:

: C₆₉H₇₅NO₁₅

: 497869-66-6
3-trifluoroacetamidopropyl (2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: 96 percent / DBU / CH₂Cl₂ / 0.25 h / 0 °C

2.1: 69 percent / BF₃*Et₂O / diethyl ether / 20 °C

3.1: 100 percent / aq. CF₃COOH / CH₂Cl₂ / 0.5 h / 0 °C

4.1: Bu₂SnO / toluene / 3 h / Heating

4.2: tetrabutylammonium iodide / toluene / Heating

With boron trifluoride diethyl etherate; di(n-butyl)tin oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; In diethyl ether; dichloromethane; toluene;
DOI:10.1039/b205684d

Reference yield:

: 497869-64-4
O-(2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-mannopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α,β-L-rhamnopyranosyl trichloroacetamidate

: 497869-66-6
3-trifluoroacetamidopropyl (2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 69 percent / BF₃*Et₂O / diethyl ether / 20 °C

2.1: 100 percent / aq. CF₃COOH / CH₂Cl₂ / 0.5 h / 0 °C

3.1: Bu₂SnO / toluene / 3 h / Heating

3.2: tetrabutylammonium iodide / toluene / Heating

With boron trifluoride diethyl etherate; di(n-butyl)tin oxide; trifluoroacetic acid; In diethyl ether; dichloromethane; toluene;
DOI:10.1039/b205684d