1-(2-Hydroxy-5-methoxy-3-nitro-phenyl)-3-(3-nitro-phenyl)-propane-1,3-dione

Base Information

Chemical Name:1-(2-Hydroxy-5-methoxy-3-nitro-phenyl)-3-(3-nitro-phenyl)-propane-1,3-dione
CAS No.:1026353-42-3
Molecular Formula:C₁₆H₁₂N₂O₈
Molecular Weight:360.28
Hs Code.:

Synonyms:1-(2-Hydroxy-5-methoxy-3-nitro-phenyl)-3-(3-nitro-phenyl)-propane-1,3-dione

Suppliers and Price of 1-(2-Hydroxy-5-methoxy-3-nitro-phenyl)-3-(3-nitro-phenyl)-propane-1,3-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-Hydroxy-5-methoxy-3-nitro-phenyl)-3-(3-nitro-phenyl)-propane-1,3-dione

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Technology Process of 1-(2-Hydroxy-5-methoxy-3-nitro-phenyl)-3-(3-nitro-phenyl)-propane-1,3-dione

There total 2 articles about 1-(2-Hydroxy-5-methoxy-3-nitro-phenyl)-3-(3-nitro-phenyl)-propane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 705-15-7
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

: 1026353-42-3
1-(2-Hydroxy-5-methoxy-3-nitro-phenyl)-3-(3-nitro-phenyl)-propane-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / nitric acid, glacial acetic acid / 2 h / Ambient temperature

2: 1.) lithium bis(trimethylsilyl)amide / 1.) THF, 078 deg C, 2 h, 2.) THF, a) -78 deg C, 1 h, b) RT, 20 h

With nitric acid; acetic acid; lithium hexamethyldisilazane;
DOI:10.1021/jm00046a020

Reference yield:

: 90564-25-3
1-(2-hydroxy-5-methoxy-3-nitrophenyl)ethanone

: 121-90-4
m-nitrobenzoic acid chloride

: 1026353-42-3
1-(2-Hydroxy-5-methoxy-3-nitro-phenyl)-3-(3-nitro-phenyl)-propane-1,3-dione

Guidance literature:: With lithium hexamethyldisilazane; Multistep reaction; 1.) THF, 078 deg C, 2 h, 2.) THF, a) -78 deg C, 1 h, b) RT, 20 h;
DOI:10.1021/jm00046a020

Reference yield:

: 1026353-42-3
1-(2-Hydroxy-5-methoxy-3-nitro-phenyl)-3-(3-nitro-phenyl)-propane-1,3-dione

: 6-methoxy-3',8-diaminoflavone

Guidance literature:: Multi-step reaction with 2 steps

1: H₂SO₄, glacial acetic acid / 1.5 h / 115 - 120 °C

2: hydrogen / 5percent Pd/C / tetrahydrofuran / 20 h / 2068.6 Torr

With sulfuric acid; hydrogen; acetic acid; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/jm00046a020