Technology Process of C38H28F6O4S4
There total 3 articles about C38H28F6O4S4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4,4,4-trifluorobutyric acid;
With
dmap; 2-methyl-6-nitrobenzoic anhydride; triethylamine;
In
dichloromethane;
for 0.333333h;
C30H22O2S4;
In
tetrahydrofuran; dichloromethane;
for 20h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 - -20 °C / Inert atmosphere
1.2: 0.5 h / Inert atmosphere
2.1: tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere
3.1: dmap; 2-methyl-6-nitrobenzoic anhydride; triethylamine / dichloromethane / 0.33 h
3.2: 20 h
With
dmap; n-butyllithium; 2-methyl-6-nitrobenzoic anhydride; triethylamine;
In
tetrahydrofuran; hexane; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere
2.1: dmap; 2-methyl-6-nitrobenzoic anhydride; triethylamine / dichloromethane / 0.33 h
2.2: 20 h
With
dmap; 2-methyl-6-nitrobenzoic anhydride; triethylamine;
In
tetrahydrofuran; dichloromethane;