1-Br-4-(Si(CH₂CHCH₂)2Me)-C₆H₄

Base Information

Chemical Name:1-Br-4-(Si(CH₂CHCH₂)2Me)-C₆H₄
CAS No.:1292360-27-0
Molecular Formula:C₁₃H₁₇BrSi
Molecular Weight:281.267
Hs Code.:

1-Br-4-(Si(CH<sub>2</sub>CHCH<sub>2</sub>)2Me)-C<sub>6</sub>H<sub>4</sub>

Synonyms:1-Br-4-(Si(CH₂CHCH₂)2Me)-C₆H₄

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Chemical Property of 1-Br-4-(Si(CH₂CHCH₂)2Me)-C₆H₄

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Technology Process of 1-Br-4-(Si(CH₂CHCH₂)2Me)-C₆H₄

There total 2 articles about 1-Br-4-(Si(CH₂CHCH₂)2Me)-C₆H₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 18141-19-0
(4-bromophenyl)(dichloro)(methyl)silane

: 106-95-6
allyl bromide

: 1292360-27-0
1-Br-4-(Si(CH₂CHCH₂)2Me)-C₆H₄

Guidance literature:: allyl bromide; With magnesium; In diethyl ether; for 10h; Inert atmosphere;

(4-bromophenyl)(dichloro)(methyl)silane; In diethyl ether; for 7h; Reflux; Inert atmosphere;
DOI:10.1016/j.jorganchem.2011.01.006

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 1292360-27-0
1-Br-4-(Si(CH₂CHCH₂)2Me)-C₆H₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium / diethyl ether / 25 h / 25 °C / Reflux; Inert atmosphere

1.2: 6.5 h / Reflux; Inert atmosphere

2.1: magnesium / diethyl ether / 10 h / Inert atmosphere

2.2: 7 h / Reflux; Inert atmosphere

With magnesium; In diethyl ether;
DOI:10.1016/j.jorganchem.2011.01.006

Reference yield: 86.0%

: 1292360-27-0
1-Br-4-(Si(CH₂CHCH₂)2Me)-C₆H₄

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1609152-74-0
4-diallylmethylsilylbenzaldehyde

Guidance literature:: 1-Br-4-(Si(CH₂CHCH₂)2Me)-C₆H₄; With tert.-butyl lithium; In diethyl ether; pentane; at -78 ℃; for 1h; Schlenk technique; Inert atmosphere;

N,N-dimethyl-formamide; In tetrahydrofuran; at 0 ℃; for 0.25h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c3dt53535e